Rubber Composition Using Composite Silica for Tire Performance

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Solution Overview

Problem

Conventional rubber compositions for tires containing silica treated with silane coupling agents do not adequately enhance rubber physical properties such as modulus, fracture characteristics, low heat build-up, abrasion resistance, and impact resilience.

Innovation Solution

A rubber composition comprising a diene rubber and a composite silica produced by polymerizing a block copolymer in the presence of silica, where the block copolymer has a first block with a (meth)acrylate having a hydroxyl group and a second block of styrene or isoprene derivatives, which covers the silica surface, improving compatibility and flexibility.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Stability of the object's composition

If silica is surface-treated with a silane coupling agent to improve dispersibility, then the dispersibility of silica in rubber composition is improved, but the rubber physical properties (modulus, fracture characteristics, low heat build-up, abrasion resistance, impact resilience) deteriorate

Engineering Contradiction:
Improvedispersibility of silicaVSAvoidrubber physical properties
Core Design Contradiction:
Stability of the object's compositionVSStrength

Solution Approach 1:

The patent introduces a block copolymer as an intermediary substance between silica and rubber. The copolymer contains a first block that interacts with silica surface and a second block that is compatible with rubber matrix, mediating the interface between filler and polymer to achieve both good dispersibility and maintained physical properties

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent uses composite silica particles consisting of silica core coated with block copolymer. This composite structure combines the dispersibility benefits of surface treatment with the mechanical property benefits of compatible polymer coating, resolving the contradiction between dispersibility and strength

Inventive Principle:
Principle #40Composite materials

2Stability of the object's composition

If silane coupling agents are used to treat silica, then the compatibility of silica with rubber is improved, but the flexibility and stretching capability of rubber deteriorate

Engineering Contradiction:
Improvecompatibility of silica with rubberVSAvoidflexibility and stretching capability
Core Design Contradiction:
Stability of the object's compositionVSDuration of action of moving object

Solution Approach 1:

The patent changes the chemical and physical parameters of the silica surface by coating with block copolymer instead of using silane coupling agents. The copolymer coating modifies surface properties to achieve compatibility while maintaining flexibility, as the polymer coating can deform with the rubber matrix during stretching

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The rubber composition achieves excellent rubber physical properties, including low rolling resistance, improved abrasion resistance, and enhanced fracture characteristics, even when using reduced amounts of silica or silane coupling agents.

Implementation Method 1

the first block covers a surface of the silica

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

a first block obtained by polymerizing a first monomer containing at least a (meth)acrylate having a hydroxyl group

Methodology Applied
Scientific EffectPolymerization: Photopolymerisation

Data Source

PatentEP3029098B1Rubber composition for tires, and pneumatic tire manufactured using same
Publication Date: 2018.01.31 TOHOKU TECHNO ARCH CO LTD
  • EP3029098B1 patent drawingFigure 1~2
  • EP3029098B1 patent drawingFigure 3~4
  • EP3029098B1 patent drawing

AI summary

An object of the present invention is to provide a rubber composition for a tire having excellent rubber physical properties. The present invention is a rubber composition for a tire comprising: a diene rubber; and a composite silica comprising a block copolymer and silica, the block copolymer comprising a first block obtained by polymerizing a first monomer containing at least a (meth)acrylate having a hydroxyl group and a second block obtained by polymerizing at least one type of a second monomer selected from the group consisting of styrene, derivatives thereof, and isoprene; the composite silica being produced in an organic solvent in the presence of the silica; and an amount of the composite silica being from 10 to 200 parts by mass per 100 parts by mass of the diene rubber; and a pneumatic tire using the same.