Ruthenium Seed Layer for Void-Free Copper ULSI Interconnects

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Solution Overview

Problem

Existing methods for forming copper seed layers for ULSI micro-interconnects face challenges such as insufficient adhesion, non-uniform plating, high impurity levels, and the need for multiple layers, which hinder the formation of uniform and void-free interconnects with low organic impurities.

Innovation Solution

A ruthenium electroplating layer is formed on a barrier layer, serving as a seed layer for copper electroplating, which ensures uniform thickness, low impurity levels, and eliminates the need for additional catalyst layers, thereby enhancing barrier properties and achieving uniform coverage on inner sidewalls and surfaces.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If electroless copper plating is used to form a seed layer on a barrier layer, then copper deposition can be achieved, but the adhesion is insufficient and the plating is non-uniform

Engineering Contradiction:
Improveadhesion of plating filmVSAvoiduniformity of plating
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

A ruthenium layer is introduced as an intermediate layer between the barrier layer and the copper electroplating layer. This ruthenium layer serves as a mediator that provides both adhesion to the barrier layer and a suitable surface for uniform copper electroplating, resolving the contradiction between adhesion and plating uniformity

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention uses a composite structure consisting of multiple layers (barrier layer + ruthenium layer + copper electroplating layer) to achieve properties that individual layers cannot provide alone. The ruthenium layer combines adhesion properties with electroplating suitability, while the copper layer provides the conductive interconnect material

Inventive Principle:
Principle #40Composite materials

2Manufacturing precision

If a catalyst metal layer is formed before the barrier layer to enable uniform electroless plating, then plating uniformity improves, but the film thickness increases and impurity levels rise

Engineering Contradiction:
Improveuniformity of platingVSAvoidfilm thickness
Core Design Contradiction:
Manufacturing precisionVSQuantity of substance

Solution Approach 1:

The invention extracts and eliminates the catalyst metal layer from the structure by using copper electroplating instead of electroless plating. The ruthenium layer alone serves as the seed layer, removing the need for the additional catalyst layer and its associated impurities while maintaining plating uniformity

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The ruthenium layer serves as a disposable seed layer that enables uniform electroplating but is not retained in the final structure. It performs its function of enabling uniform copper deposition and then serves as part of the barrier system, eliminating the need for permanent catalyst layer inclusion

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Quantity of substance

If CVD or ALD is used to form films with low impurity levels, then film purity improves, but organic impurities exceed 100 wt ppm and resistance increases

Engineering Contradiction:
Improveimpurity concentrationVSAvoidelectrical resistance
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The invention replaces chemical vapor deposition (CVD) and atomic layer deposition (ALD) processes with physical vapor deposition (PVD) sputtering for forming the barrier and ruthenium layers. This substitution eliminates organic impurities introduced by chemical processes while maintaining excellent film quality and low electrical resistance

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The invention changes the deposition method parameter from chemical processes (CVD/ALD) to physical processes (sputtering). This parameter change fundamentally alters the impurity profile by eliminating carbon-containing organic impurities while maintaining controlled film properties through physical deposition mechanisms

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The ruthenium layer provides a uniform and impurity-free seed layer for copper electroplating, ensuring void-free micro-interconnects with improved barrier properties and reduced film thickness, addressing the limitations of existing methods.

Implementation Method 1

a ruthenium layer that has been formed by an electroplating process

Methodology Applied
Scientific EffectElectroplating: Electroplating

Data Source

PatentUS8390123B2ULSI micro-interconnect member having ruthenium electroplating layer on barrier layer
Publication Date: 2013.03.05 JX NIPPON MINING & METALS CORP

AI summary

A ULSI micro-interconnect member having a substrate and a ULSI micro-interconnect formed on the substrate, wherein the ULSI micro-interconnect includes a barrier layer formed on the substrate and a ruthenium electroplating layer formed on the barrier layer; the ULSI micro-interconnect member further including a copper electroplating layer formed using the ruthenium electroplating layer as a seed layer; and a process for fabricating the ULSI micro-interconnect members.