Salt-Free Antibody Formulations for Low Viscosity

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Solution Overview

Problem

Current protein and antibody formulations face challenges with high viscosity, osmolality, and protein aggregation, which complicates processing and administration, especially for subcutaneous injections, and requires a balance of stabilizers to maintain stability and osmolality without causing injection pain.

Innovation Solution

Development of low viscosity, substantially isosmotic antibody and protein formulations without inorganic salts, using histidine, sugars, and non-ionic surfactants like polysorbate, which maintain stability and osmolality, allowing for increased concentrations of stabilizers and reduced injection pain, and are suitable for both liquid and lyophilized forms.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If high protein concentration is used in antibody formulations, then dosage volume is reduced and stability is improved, but viscosity increases significantly making processing and injection difficult

Engineering Contradiction:
Improveprotein concentrationVSAvoidviscosity
Core Design Contradiction:
Quantity of substanceVSEase of operation

Solution Approach 1:

The patent changes the chemical composition parameters of the formulation by introducing specific excipients (histidine buffer at pH 5.0-6.0, non-ionic surfactants like polysorbate 80, and sugar alcohols like mannitol or sorbitol) to modify the physical properties of the protein solution, thereby reducing viscosity while maintaining high protein concentration

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite formulation system combining protein, buffer, surfactant, and sugar alcohol components that work synergistically to maintain solubility and reduce viscosity at high concentrations, enabling both high dosage strength and ease of administration

Inventive Principle:
Principle #40Composite materials

2Stability of the object's composition

If high concentrations of stabilizers are added to maintain protein stability, then protein aggregation is reduced, but osmolality increases causing injection pain and tissue damage

Engineering Contradiction:
Improveprotein stabilityVSAvoidinjection pain
Core Design Contradiction:
Stability of the object's compositionVSObject-affected harmful factors

Solution Approach 1:

The patent changes the type of stabilizer used from traditional high-osmolality agents to sugar alcohols (mannitol, sorbitol) that provide stabilization with lower osmolality contribution, and adjusts pH to 5.0-6.0 to optimize protein stability while controlling osmolality

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses sugar alcohols as temporary stabilizing agents that fulfill their protective function during storage and administration, after which they are safely metabolized or excreted, providing stable protection without long-term osmolality issues

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Ease of operation

If liquid formulation is used for convenience of administration, then ease of injection is improved, but protein aggregation and phase separation occur at high concentrations

Engineering Contradiction:
Improveease of administrationVSAvoidphase separation
Core Design Contradiction:
Ease of operationVSStability of the object's composition

Solution Approach 1:

The patent adjusts multiple formulation parameters including pH (5.0-6.0), ionic strength, and excipient concentrations to shift the phase behavior of the protein solution, ensuring that the liquid formulation remains stable and monophasic at high protein concentrations suitable for convenient administration

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent introduces non-ionic surfactants as intermediary substances that mediate between protein molecules, preventing aggregation and phase separation while maintaining the liquid state and ease of administration

Inventive Principle:
Principle #24Intermediary (Mediator)

Data Source

PatentEP3117837B1Antibody formulations
Publication Date: 2019.05.22 BAYER HEALTHCARE LLC
  • EP3117837B1 patent drawingFigure 1
  • EP3117837B1 patent drawingFigure 2
  • EP3117837B1 patent drawing

AI summary

Provided are salt-free antibody and other protein formulations that are substantially isosmotic and of low viscosity. Also provided are methods for the treatment of diseases using the disclosed formulations.