SAM Regeneration Pathway Using Formic Acid for Faster Methylation

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing methods for recycling S-adenosylmethionine (SAM) do not sufficiently accelerate the methylation reaction and are inefficient in producing methyl compounds.

Innovation Solution

A method utilizing formic acid or its salts to regenerate SAM by converting formaldehyde to formic acid, followed by a series of enzymatic reactions involving formate-tetrahydrofolate ligase, methenyl-tetrahydrofolate cyclohydrolase, and other enzymes to produce 5-methyltetrahydrofolate, which is then used to regenerate SAM and produce methyl compounds.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If methanol is added to a culture medium of a microorganism coexpressing methylase and methanol dehydrogenase to recycle SAM, then SAM can be regenerated, but the methylation reaction is not sufficiently accelerated

Engineering Contradiction:
ImproveSAM regenerationVSAvoidmethylation reaction rate
Core Design Contradiction:
Quantity of substanceVSProductivity

Solution Approach 1:

The invention changes the carbon source parameter from methanol to formic acid, and introduces a multi-enzyme system (FtfL, Fch, MtdA, MetF) to convert formic acid through formate-tetrahydrofolate ligase, methenyl-tetrahydrofolate cyclohydrolase, methylene-tetrahydrofolate dehydrogenase, and 5,10-methylene-tetrahydrofolate reductase pathways. This parameter change and enzyme system introduction significantly accelerates the methylation reaction while maintaining SAM regeneration

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention introduces formic acid as an intermediary substance that is converted to formate, then to 5-methyltetrahydrofolate, which serves as a methyl group donor to regenerate SAM. This intermediary pathway (formic acid → formate → 5-methyl-THF → SAM) provides an efficient route that accelerates the overall methylation reaction compared to direct methanol addition

Inventive Principle:
Principle #24Intermediary (Mediator)

2Quantity of substance

If formaldehyde dehydrogenase activity is reduced to suppress conversion of formaldehyde to formic acid, then SAM recycling is improved, but the overall efficiency of methyl compound production is insufficient

Engineering Contradiction:
ImproveSAM recyclingVSAvoidmethyl compound production efficiency
Core Design Contradiction:
Quantity of substanceVSProductivity

Solution Approach 1:

Instead of suppressing formaldehyde to formic acid conversion (the conventional approach), the invention inverts the pathway by directly supplying formic acid as the starting material and using a controlled multi-enzyme system to convert it to 5-methyltetrahydrofolate and then to SAM. This inverted approach avoids the need to suppress formaldehyde dehydrogenase while achieving efficient SAM recycling and methyl compound production

Inventive Principle:
Principle #13The other way round (Inversion)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method efficiently regenerates SAM and accelerates the methylation reaction, enhancing the production of methyl compounds.

Implementation Method 1

the production of 5-methyltetrahydrofolate from formic acid or a salt thereof and tetrahydrofolate is performed in the presence of formate-tetrahydrofolate ligase (FtfL)

Methodology Applied
Scientific EffectEnzyme catalysis: Enzyme

Implementation Method 2

methenyl-tetrahydrofolate cyclohydrolase (Fch)

Methodology Applied
Scientific EffectEnzyme catalysis: Enzyme

Implementation Method 3

methylene-tetrahydrofolate dehydrogenase (MtdA)

Methodology Applied
Scientific EffectDehydrogenation: Redox Reactions

Implementation Method 4

5,10-methylene-tetrahydrofolate reductase (MetF)

Methodology Applied
Scientific EffectReduction: Reduction

Implementation Method 5

the conversion of S-adenosylhomocysteine to homocysteine is performed in the presence of S-adenosylhomocysteine nucleosidase (Mtn) and S-ribosylhomocysteine lyase (LuxS)

Methodology Applied
Scientific EffectEnzyme catalysis: Enzyme

Implementation Method 6

the production of methionine by transferring a methyl group of the 5-methyltetrahydrofolate to the homocysteine is performed in the presence of methionine synthase (MetH or MetE)

Methodology Applied
Scientific EffectMethyl group transfer: Enzyme

Implementation Method 7

the conversion of the methionine to S-adenosylmethionine is performed in the presence of methionine adenosyltransferase (MetK)

Methodology Applied
Scientific EffectEnzyme catalysis: Enzyme

Implementation Method 8

the conversion of methanol to formaldehyde is performed in the presence of methanol dehydrogenase (Medh) and/or methanol oxidase (Mox)

Methodology Applied
Scientific EffectOxidation: Oxidation

Implementation Method 9

the conversion of formaldehyde to formic acid is performed in the presence of formaldehyde dehydrogenase (FdhA)

Methodology Applied
Scientific EffectDehydrogenation: Redox Reactions

Data Source

PatentEP4692363A1Method for producing methyl compound
Publication Date: 2026.02.11 MITSUBISHI CHEM CORP
  • EP4692363A1 patent drawingFigure 1
  • EP4692363A1 patent drawingFigure 2
  • EP4692363A1 patent drawing

AI summary

An object of the present invention is to provide a method for producing a methyl compound. The present invention provides a method for producing a methyl compound using formic acid.