Super Absorbent Polymer Reassembly for Granulation and Drying Balance

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Solution Overview

Problem

Existing methods for preparing super absorbent polymers face challenges in improving drying efficiency, reducing the generation of re-fines, and enhancing absorption performance, particularly under pressure and permeability, due to issues with granulation strength and moisture content during the reassembly process.

Innovation Solution

A method involving the preparation of a hydrogel polymer through polymerization, followed by classification, mixing with a polycarboxylic acid-based copolymer and water, extrusion, and surface cross-linking, with controlled water usage to optimize granulation strength and reduce re-fines, thereby improving absorption performance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If the amount of water used in the reassembly process is increased, then granulation strength is improved, but energy consumption during drying increases and costs increase

Engineering Contradiction:
Improvegranulation strengthVSAvoidenergy consumption during drying
Core Design Contradiction:
StrengthVSUse of energy by moving object

Solution Approach 1:

The patent applies parameter changes by optimizing the water content in the fine reassembly to a specific range (5-20% by weight) rather than using excessive amounts. This controlled parameter adjustment achieves sufficient granulation strength while minimizing the energy required for subsequent drying, thereby resolving the contradiction between strength improvement and energy consumption.

Inventive Principle:
Principle #35Parameter changes

2Use of energy by moving object

If the amount of water used in the reassembly process is reduced, then energy consumption during drying is reduced, but cohesive strength is lowered and reassembly is not performed properly

Engineering Contradiction:
Improveenergy consumption during dryingVSAvoidcohesive strength
Core Design Contradiction:
Use of energy by moving objectVSStrength

Solution Approach 1:

The patent resolves this contradiction by precisely controlling the water content parameter within the optimal range of 5-20% by weight. This controlled parameter change provides sufficient moisture for proper reassembly and cohesive strength formation while avoiding excessive water that would require high energy for drying, thus achieving both low energy consumption and adequate cohesive strength.

Inventive Principle:
Principle #35Parameter changes

3Strength

If the amount of water used in the reassembly process is increased, then granulation strength is improved, but the load on the device for preparing super absorbent polymer increases

Engineering Contradiction:
Improvegranulation strengthVSAvoidmoisture content
Core Design Contradiction:
StrengthVSQuantity of substance

Solution Approach 1:

The patent applies parameter changes by limiting the water content to an optimal range (5-20% by weight) rather than using excessive amounts. This controlled parameter adjustment achieves the necessary granulation strength for proper particle formation while minimizing the total moisture content that would otherwise increase the load on processing equipment.

Inventive Principle:
Principle #35Parameter changes

4Strength

If additional extrusion process is performed on fine reassembly with low moisture content, then granulation strength is improved and re-fines are reduced, but process complexity increases

Engineering Contradiction:
Improvegranulation strengthVSAvoidprocess complexity
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The patent applies preliminary action by performing the extrusion process during the reassembly operation itself, rather than as a separate subsequent step. This integrated approach allows the extrusion to shape and strengthen the particles while they are still moist and pliable, achieving granulation strength improvement without requiring additional separate processing equipment or steps.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method enhances drying efficiency, reduces re-fine generation, and improves absorption under pressure and permeability of the final super absorbent polymer by controlling granulation strength during the reassembly process.

Implementation Method 1

water absorbency of the super absorbent polymer depends on the affinity and molecular expansion, and an absorption rate is largely dependent on the osmotic pressure of the absorbent polymer itself

Methodology Applied
Scientific EffectOsmotic pressure: Osmosis

Implementation Method 2

A super absorbent polymer (SAP) is a type of synthetic polymeric material capable of absorbing 500 to 1000 times its own weight of moisture

Methodology Applied
Scientific EffectAbsorption: Absorption (physical)

Implementation Method 3

molecular expansion due to repulsion between polymer electrolyte ions

Methodology Applied
Scientific EffectMolecular expansion:

Implementation Method 4

inhibition of expansion due to cross-linking

Methodology Applied
Scientific EffectCross-linking:

Implementation Method 5

the amount of energy used during a drying process of the fine reassembly increases

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentUS12528072B2Method for preparing super absorbent polymer
Publication Date: 2026.01.20 LG CHEM LTD
  • US12528072B2 patent drawing
  • US12528072B2 patent drawing
  • US12528072B2 patent drawing

AI summary

The present disclosure relates to a method for preparing a super absorbent polymer. More specifically, it relates to a method for preparing a super absorbent polymer capable of improving drying efficiency, reducing a generation amount of re-fines, and simultaneously improving absorption performance, in particular, absorption under pressure and permeability of the finally prepared super absorbent polymer by controlling granulation strength of the extruded fine reassembly.