Seal Validation Using Chemical Pre-treatment

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Solution Overview

Problem

Existing methods for validating seals for use in extreme subsea or subterranean environments are time-consuming and expensive, failing to effectively address the long-term behavior of seals in permanent installations, particularly in high-pressure and chemically challenging conditions.

Innovation Solution

A method involving chemical pre-treatment of seals to approximate end-of-life conditions, using material samples to develop an Arrhenius response curve, determining pre-treatment time and temperature based on this curve, and then performing validation tests on the pre-treated seals to evaluate their performance at end-of-life, reducing the need for extensive testing.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If traditional seal validation testing procedures are used to evaluate long-term seal behavior, then accurate estimates of total seal life and long-term behavior are obtained, but the testing process becomes time-consuming and expensive

Engineering Contradiction:
Improveseal life estimation accuracyVSAvoidtesting duration
Core Design Contradiction:
ReliabilityVSLoss of time

Solution Approach 1:

The patent applies preliminary action by exposing seals to accelerated chemical degradation conditions before final validation testing. This pre-treatment step simulates long-term chemical exposure effects in advance, allowing the seal's end-of-life behavior to be evaluated without requiring years of actual service testing. The accelerated chemical exposure creates artificial aging that correlates with long-term performance, thus obtaining reliable seal life estimates in a compressed time frame.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent utilizes parameter changes by modifying the chemical exposure conditions to accelerate degradation. By changing parameters such as chemical concentration, temperature, and exposure duration in the pre-treatment phase, the seal undergoes accelerated aging that mimics years of service in a much shorter period. This allows the validation process to capture long-term behavior patterns without requiring correspondingly long test durations.

Inventive Principle:
Principle #35Parameter changes

2Reliability

If traditional seal validation testing procedures are used to evaluate long-term seal behavior, then accurate estimates of total seal life and long-term behavior are obtained, but the testing cost increases

Engineering Contradiction:
Improveseal life estimation accuracyVSAvoidtesting cost
Core Design Contradiction:
ReliabilityVSLoss of energy

Solution Approach 1:

The pre-treatment step performs the costly and time-consuming chemical degradation simulation in advance under controlled accelerated conditions. By completing the equivalent of years of chemical exposure in a short pre-treatment phase, the subsequent validation testing requires minimal additional resources, dramatically reducing overall testing costs while maintaining accuracy in seal life estimation.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent skips the intermediate years of actual service testing by rushing through the degradation process in the pre-treatment phase using accelerated chemical exposure. This allows the validation to jump directly to evaluating end-of-life behavior without waiting for the seal to naturally age over years, thereby eliminating the time and cost associated with long-term field testing.

Inventive Principle:
Principle #21Skipping (Rushing through)

3Reliability

If seals are tested in high-pressure and chemically challenging subsea or subterranean environments, then realistic performance data is obtained, but the testing complexity and difficulty increase

Engineering Contradiction:
Improveseal performance data realismVSAvoidtesting system complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent segments the validation process into distinct phases: a pre-treatment phase that handles the complex chemical degradation separately under controlled conditions, and a final validation phase that tests mechanical performance. This segmentation allows the complex chemical exposure to be managed independently and systematically, reducing the overall complexity of the testing system while maintaining realism in the performance data obtained.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The pre-treatment process acts as an intermediary that prepares the seal for final validation by pre-exposing it to accelerated chemical conditions. This intermediary step decouples the complex chemical degradation process from the mechanical validation testing, allowing each to be optimized and controlled separately. The pre-treated seal then undergoes simpler mechanical testing that focuses purely on performance evaluation without the confounding variables of ongoing chemical exposure.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach provides valuable information on seal performance at end-of-life conditions more cost-effectively and efficiently than traditional methods, without the need for lengthy testing procedures, offering a low-cost and time-saving validation process.

Implementation Method 1

downhole equipment lowered through the well is often exposed to various chemicals during well completion and production operations

Methodology Applied
Scientific EffectChemical degradation: Chemical Bonding

Implementation Method 2

determining an Arrhenius relationship between a material property of the material samples and temperature

Methodology Applied
Scientific EffectArrhenius relationship:

Data Source

PatentUS11543372B2Seal validation with chemical pre-treatment
Publication Date: 2023.01.03 INNOVEX INTERNATIONAL INC
  • US11543372B2 patent drawing
  • US11543372B2 patent drawing
  • US11543372B2 patent drawing

AI summary

Methods for performing seal validation with a chemical pre-treatment are provided. One such method includes establishing an Arrhenius relationship between a material property response of a material exposed to a test fluid based on experimental results of testing a plurality of material samples made of the material across multiple temperatures. The method also includes determining, based on the Arrhenius relationship, a pre-treatment time and a pre-treatment temperature that approximates a seal end-of-life condition. The method further includes pre-treating a seal by exposing the seal to the test fluid at the determined pre-treatment temperature for the determined pre-treatment time, the seal having at least in part a same material composition as the plurality of material samples, and after pre-treating the seal, performing one or more validation tests on the pre-treated seal.