Segmented Bleach Adjunct Particles for Detergent Spotting

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Solution Overview

Problem

Large particle detergent formulations often exhibit localized spotting and dye damage, particularly when using smaller bleach particles, which are not effectively addressed by existing technologies.

Innovation Solution

A bleach adjunct particle with specific dimensions and composition, comprising phthalimido-peroxy-hexanoic-acid (PAP) dispersed in a water-soluble material carrier, is combined with a coated detergent particle to minimize spotting and dye damage, where the bleach adjunct particle is uncoated and the detergent particle is coated with surfactants and inorganic salts, both having similar shapes and sizes.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If smaller bleach particles are used in detergent formulations, then the bleach is more effective at removing stains, but localized spotting and dye damage occur on fabrics

Engineering Contradiction:
Improvestain removal effectivenessVSAvoidlocalized spotting and dye damage
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The detergent product is segmented into two distinct particle size populations: large particles (0.5-2mm) serving as the detergent base and small particles (10-200 microns) containing the bleach adjunct. This segmentation allows the bleach to be delivered in controlled micro-doses through the larger detergent particles, preventing concentrated bleach contact that causes spotting while maintaining effective stain removal capability.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The bleach adjunct particles are locally embedded within or associated with specific regions of the larger detergent particles. This local quality ensures that bleach is released only where and when needed during the wash cycle, rather than being uniformly distributed, thereby preventing localized spotting while maintaining effective stain removal at targeted locations.

Inventive Principle:
Principle #3Local quality

2Object-affected harmful factors

If larger detergent particles are used to reduce spotting, then fabric damage is minimized, but bleach effectiveness is reduced

Engineering Contradiction:
Improvefabric spotting and damageVSAvoidbleach effectiveness
Core Design Contradiction:
Object-affected harmful factorsVSReliability

Solution Approach 1:

The small bleach-containing particles are nested within or associated with the larger detergent particles, creating a hierarchical structure where the large particles serve as carriers for the small bleach particles. This nesting allows the system to benefit from both size regimes: the large particles prevent spotting by providing a gentle matrix, while the nested small particles deliver effective bleach action.

Inventive Principle:
Principle #7Nested doll (Nesting)

Solution Approach 2:

The detergent product is formulated as a composite system combining two different particle size populations with distinct functions. The large particles (0.5-2mm) provide a gentle matrix that prevents spotting, while the small particles (10-200 microns) containing bleach adjunct provide effective stain removal, creating a synergistic composite material that overcomes the limitations of using either particle size alone.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution significantly reduces spotting and dye damage compared to smaller particle formulations, as demonstrated by reduced color change in dye damage assessments and minimized fabric damage during washing.

Implementation Method 1

wherein when 1 gm of the bleach adjunct particle is dissolved in 100 ml of demineralised water the pH to the solution is in the range from 3 to 6

Methodology Applied
Scientific EffectAqueous dissolution: Solvation

Implementation Method 2

from 5 to 60 wt % dispersed in the composition susceptible to aqueous attack particles of PAP

Methodology Applied
Scientific EffectDispersal: Dispersion (of waves)

Data Source

PatentEP3320076B1Large particles
Publication Date: 2019.01.02 UNILEVER PLC

AI summary

The present invention large bleaching particle adjunct to use with similar sized detergent particles.