Segmented Distillation Column Cells for Energy Efficiency

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Solution Overview

Problem

Large-scale distillation processes are energy-intensive, leading to stability and cost issues due to the need for tall columns and inefficient energy use in existing distillation devices, particularly in distributing a two-phase liquid/steam mixture across evaporator stages.

Innovation Solution

A distillation device with three or more cells arranged vertically in the column bottom for multi-stage heating and partial evaporation, allowing for independent heating and partial evaporation of liquid streams using suitable energy sources, with partial returns of liquid between cells to optimize energy use and reduce column height.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If the bottom liquid is heated in several stages using evaporators connected in series vertically, then the separation efficiency is improved, but the column height increases leading to stability problems and higher costs

Engineering Contradiction:
Improveseparation efficiencyVSAvoidcolumn height
Core Design Contradiction:
Manufacturing precisionVSLength of stationary object

Solution Approach 1:

The column bottom is segmented into multiple cells (first cell, second cell, third cell) that are arranged horizontally adjacent to each other rather than vertically stacked. Each cell contains evaporator stages, allowing multi-stage heating to occur in a horizontal sequence. This segmentation maintains the separation efficiency of multi-stage heating while avoiding the stability issues associated with tall vertical columns.

Inventive Principle:
Principle #1Segmentation

2Length of stationary object

If evaporator stages are arranged horizontally one behind the other, then the column height is reduced, but the distribution of two-phase liquid/steam mixture becomes problematic

Engineering Contradiction:
Improvecolumn heightVSAvoiddistribution of two-phase mixture
Core Design Contradiction:
Length of stationary objectVSEase of operation

Solution Approach 1:

A liquid distributor is introduced as an intermediary device between the evaporator stages in the horizontal arrangement. This distributor ensures proper distribution of the two-phase liquid/steam mixture from one evaporator stage to the next, solving the distribution problem that arises in horizontal configurations while maintaining the advantage of reduced column height.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Loss of energy

If existing energy sources are used for individual evaporator stages, then energy costs are reduced, but the device complexity increases

Engineering Contradiction:
Improveenergy costsVSAvoiddevice complexity
Core Design Contradiction:
Loss of energyVSDevice complexity

Solution Approach 1:

The system is designed to accept multiple types of energy sources (steam, hot condensate, electrical heaters) for the evaporator stages, allowing existing energy sources from different parts of the process to be utilized. This multi-functionality approach enables energy recovery and reuse without requiring a completely new energy supply system, thus reducing energy costs while limiting complexity increases.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This design enhances energy efficiency, reduces energy costs, and prevents stability issues by allowing for the use of existing energy sources, achieving effective separation of substances while maintaining column stability and reducing height.

Implementation Method 1

multi-stage heating and partial evaporation of the liquid flowing through the cells

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 2

each obtaining a partially evaporated stream (4,5)

Methodology Applied
Scientific EffectPartial evaporation: Evaporation

Implementation Method 3

separating a feed stream (1) into a top product stream (2), a bottom product stream (3)

Methodology Applied
Scientific EffectDistillation: Distillation

Implementation Method 4

The bottom stream from the first cell (I) in the flow direction is withdrawn in liquid form and applied to a heat exchanger (WT1), in which the stream is heated

Methodology Applied
Scientific EffectHeat transfer: Heat Exchanger

Data Source

PatentEP3316981B1Distillation device comprising a column which has three or a plurality of cells in series through which fluid flows and method for distilling or extractive distillation by use of the distillation device
Publication Date: 2020.10.21 BASF SE
  • EP3316981B1 patent drawingFigure 1
  • EP3316981B1 patent drawingFigure 1A~1B
  • EP3316981B1 patent drawingFigure 1C

AI summary

The invention relates to a distillation device comprising a column (K) for separating a feed stream (1) into a head product stream (2), a bottom product stream (3) and optionally one or more side extraction streams, having three or more cells (I, II, III) in series through which fluid flows, wherein at least the first cell is integrated into the bottom of the column (K), for multi-stage heating and partial evaporation of the liquid flowing through the cells with the exception of the liquid from the last cell in an evaporation stage.