Segmented Showerhead for Multi-Temperature Precursor Delivery

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Solution Overview

Problem

In organic vapor deposition processes, co-depositing cooler and warmer materials can lead to dissociation and condensation issues due to purity and contamination concerns, particularly when using a carrier gas, and existing technologies struggle to manage thermal cross-talk and pressure drops in multi-material deposition.

Innovation Solution

A showerhead assembly with fluidly isolated gas delivery portions, each with a wedge-shaped body and plenum, allows for simultaneous heating of multiple materials to different temperatures, preventing thermal cross-talk and ensuring uniform deposition on a substrate, while maintaining thermal isolation and reducing pressure drops.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If multiple materials are co-deposited using a conventional showerhead, then deposition efficiency is improved, but thermal cross-talk causes dissociation and condensation issues

Engineering Contradiction:
Improvedeposition efficiencyVSAvoidmaterial stability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The showerhead is divided into multiple independently controlled gas delivery portions, each capable of delivering a different material at a different temperature. This segmentation prevents thermal cross-talk between materials while maintaining the ability to deposit multiple materials simultaneously, thus resolving the contradiction between deposition efficiency and material stability.

Inventive Principle:
Principle #1Segmentation

2Manufacturing precision

If different temperatures are applied to different gas delivery portions, then material-specific deposition conditions are achieved, but pressure drops increase

Engineering Contradiction:
Improvedeposition uniformityVSAvoidpressure drop
Core Design Contradiction:
Manufacturing precisionVSStress or pressure

Solution Approach 1:

By segmenting the showerhead into separate gas delivery portions with independent temperature control, the system can apply different temperatures to different materials without causing thermal cross-talk. This segmentation allows precise control of deposition conditions for each material while managing pressure drops through independent flow control for each segment.

Inventive Principle:
Principle #1Segmentation

3Ease of operation

If carrier gas is used in organic vapor deposition, then deposition process is simplified, but purity and contamination concerns arise

Engineering Contradiction:
Improveprocess simplicityVSAvoidmaterial purity
Core Design Contradiction:
Ease of operationVSLoss of substance

Solution Approach 1:

The showerhead is segmented into separate gas delivery portions for different materials, eliminating the need for a carrier gas that would cause contamination. Each material can be delivered independently through its own segment, maintaining process simplicity while ensuring material purity and preventing contamination.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This solution enables the efficient and contamination-free co-deposition of multiple materials at varying temperatures, preventing unwanted reactions and condensation, thereby improving the purity and uniformity of deposited films in semiconductor and optical device manufacturing.

Implementation Method 1

heating a first gas delivery portion to a first temperature; and simultaneously heating a second gas delivery portion to a second temperature different than the first temperature

Methodology Applied
Scientific EffectVaporization: Evaporation

Data Source

PatentUS12043895B2Methods of using a segmented showerhead for uniform delivery of multiple pre-cursors
Publication Date: 2024.07.23 APPLIED MATERIALS INC
  • US12043895B2 patent drawing
  • US12043895B2 patent drawing
  • US12043895B2 patent drawing

AI summary

Methods of introducing precursors through a segmented showerhead are provided herein. In some embodiments, a method of introducing precursors through a segmented showerhead having a plurality of gas delivery portions that are fluidly isolated includes heating a first gas delivery portion to a first temperature; and simultaneously heating a second gas delivery portion to a second temperature different than the first temperature, wherein each of the first and second gas delivery portions (i) have a wedge shaped body that defines a plenum, (ii) are coplanar, and (iii) together form a showerhead having a circular shape.