Self-Etch Dental Adhesive Merging Etching and Bonding

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Solution Overview

Problem

Current dental bonding systems, including multiple-component, two-component, and single-component primer systems, face challenges in achieving high bond strengths and stability over time, often requiring complex procedures and resulting in moderate to low bond strengths, especially when exposed to in vivo conditions.

Innovation Solution

A one-part or two-part self-etching primer adhesive system comprising specific components such as bisphenol A diglycidylether methacrylate phosphate, 2-hydroxyethyl-methacrylate, biphenyl dimethacrylate, dipentaerythritol pentaacrylate, bisphenol A diglycidylmethacrylate, ethyl-4-dimethyl-aminobenzoate, and camphorquinone, along with deionized water, aryl sulfinate salt, and ethanol, which allows for improved penetration and bonding to dentin and enamel without the need for additional mixing or activators, enhancing bond strength and stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If multiple-component primer systems are used to achieve high bond strengths, then bond strength is improved, but device complexity and time consumption increase

Engineering Contradiction:
Improvebond strengthVSAvoidsystem complexity
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The patent combines multiple primer components (phosphate ester monomer, hydrophilic monomer, acidic monomer, cross-linking monomer, tertiary amine, and initiator) into a single self-etching adhesive composition. This merging eliminates the need for separate application steps of multiple primers while maintaining high bond strength through the synergistic interaction of all components within one formulation.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The single-component self-etching adhesive performs multiple functions simultaneously: etching the dentin surface, priming the substrate, and bonding the restorative material. The composition contains all necessary functional groups (acidic groups for etching, hydrophilic groups for penetration, polymerizable groups for bonding) within one universal formulation that replaces traditional multi-step systems.

Inventive Principle:
Principle #6Universality (Multi-functionality)

2Strength

If multiple-component primer systems are used to achieve high bond strengths, then bond strength is improved, but time consumption increases

Engineering Contradiction:
Improvebond strengthVSAvoidapplication time
Core Design Contradiction:
StrengthVSLoss of time

Solution Approach 1:

The patent combines multiple primer components (phosphate ester monomer, hydrophilic monomer, acidic monomer, cross-linking monomer, tertiary amine, and initiator) into a single self-etching adhesive composition. This merging eliminates the need for separate application steps of multiple primers while maintaining high bond strength through the synergistic interaction of all components within one formulation.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The adhesive composition is pre-formulated with all necessary components in optimal concentrations and compatibility. The phosphate ester monomer and other functional groups are already integrated and stabilized in the final product, eliminating the need for dental professionals to mix components immediately before use and reducing application time.

Inventive Principle:
Principle #10Preliminary action

3Ease of operation

If single-component primer systems are used to simplify the procedure, then ease of operation is improved, but bond strength decreases

Engineering Contradiction:
Improvesimplicity of useVSAvoidbond strength
Core Design Contradiction:
Ease of operationVSStrength

Solution Approach 1:

The patent creates a composite adhesive formulation that integrates multiple functional monomers and additives into a single component system. The composite nature of the adhesive, containing phosphate ester monomer, hydrophilic monomer, acidic monomer, cross-linking monomer, tertiary amine, and initiator, provides both simplicity of application and high bond strength through the synergistic effects of its composite composition.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent optimizes the chemical parameters of the single-component system by carefully selecting and balancing the concentrations of different monomers and additives. The phosphate ester monomer content, molecular weight, and functional group ratios are specifically adjusted to achieve both ease of operation and high bond strength, demonstrating that parameter optimization can resolve the trade-off between simplicity and performance.

Inventive Principle:
Principle #35Parameter changes

4Adaptability or versatility

If conventional adhesive systems are used, then compatibility with various composites is needed, but additional products and mixing steps are required

Engineering Contradiction:
Improvecompatibility with compositesVSAvoidnumber of products
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The self-etching adhesive is designed as a universal bonding system that is compatible with light-cured, self-cured, and dual-cured composite materials. The adhesive contains initiators and functional groups that can work with all three types of composites, eliminating the need for separate adhesive products for different composite types and simplifying the overall material system.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system achieves high microtensile shear bond strengths comparable to or exceeding those of existing systems, demonstrating improved durability and compatibility with light-cured, self-cured, and dual-cured materials, while simplifying the application process and reducing the need for additional products.

Implementation Method 1

treating the dental substrate with (1) an acidic acid solution of inorganic acids, polycarboxylic acids and metal salts of such acids capable of changing valence states

Methodology Applied
Scientific EffectAcid etching:

Implementation Method 2

displaying improved penetration into dentin and enamel, thereby forming a better hybrid layer

Methodology Applied
Scientific EffectPenetration: Permeation

Implementation Method 3

applying a second polymerizable adhesive bonding monomer to the substrate comprising PMDM, BDTA-HEMA, 4-META, or other polymerizable acidic monomers

Methodology Applied
Scientific EffectPolymerization: Photopolymerisation

Data Source

PatentUS8106110B2Dual application mode self-etch dental adhesives compatible with self-cured and dual-cured composites
Publication Date: 2012.01.31 BISCO INC

AI summary

The present application relates to a dental primer adhesive system that is capable of being used as either a one-step or two-step self-etch dental primer and is compatible with self-cure composites and dual-cure composites with reduced permeability.