Semiconductor Metallization via Self-Assembled Monolayers

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Solution Overview

Problem

Current semiconductor metallization methods introduce significant damage and defects in metal structures and dielectric layers during the formation of vias and trenches, particularly at the 7nm node technology and beyond, due to incomplete filling and etching-induced damages.

Innovation Solution

The method employs strategically placed selective self-assembled monolayers (SAMs) combined with sacrificial layers for bottom-up filling of vias and trenches, allowing for controlled metal growth and minimizing defects, and replaces sacrificial layers with low-k dielectric layers to avoid damage to the dielectric material.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional metallization methods are used to form vias and trenches, then metal structures can be created, but significant damage and defects are introduced in the metal structures and dielectric layers

Engineering Contradiction:
Improvequality of metal structuresVSAvoiddamage to dielectric layers
Core Design Contradiction:
Manufacturing precisionVSObject-affected harmful factors

Solution Approach 1:

The patent applies preliminary action by depositing self-assembled monolayers (SAMs) on the sidewalls of vias and trenches before the metal filling process. These SAMs serve as protective coatings that prevent damage to the dielectric layers during subsequent etching and filling operations, thereby resolving the contradiction between creating metal structures and avoiding damage to dielectric layers.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent uses self-assembled monolayers (SAMs) as intermediary substances between the metal filling process and the dielectric layers. These SAMs act as mediators that facilitate controlled metal deposition while protecting the underlying dielectric structures from damage, thus improving metal structure quality without compromising dielectric integrity.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Ease of manufacture

If filling proceeds from the side-walls of vias and trenches, then metal structures can be formed, but defects are unavoidable at the junction of the growth fronts

Engineering Contradiction:
Improvemetal filling processVSAvoiddefect level in metal structures
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The patent applies inversion by reversing the conventional filling approach. Instead of allowing metal to grow upward from the sidewalls (bottom-up), the method deposits metal in a top-down manner through the via/trench openings. This inverted approach eliminates the formation of growth front junctions that cause defects, while maintaining ease of manufacture through controlled deposition processes.

Inventive Principle:
Principle #13The other way round (Inversion)

Solution Approach 2:

The patent extracts the problematic sidewall growth mechanism from the filling process. By removing the sidewall-dependent growth approach and replacing it with direct top-down deposition, the method eliminates the inherent defects at growth front junctions while preserving the manufacturability of the metal filling process.

Inventive Principle:
Principle #2Taking out (Extraction)

3Manufacturing precision

If plasma etching is used to form vias and trenches, then narrow features can be created, but etching-induced damages occur in the dielectric material

Engineering Contradiction:
Improvedimensional accuracy of narrow featuresVSAvoidetching-induced damage
Core Design Contradiction:
Manufacturing precisionVSObject-affected harmful factors

Solution Approach 1:

The patent applies beforehand cushioning by depositing self-assembled monolayers (SAMs) on the dielectric surfaces before plasma etching operations. These SAMs act as protective cushioning layers that absorb etching damage, allowing precise formation of narrow vias and trenches while minimizing damage to the surrounding dielectric material.

Inventive Principle:
Principle #11Beforehand cushioning (Prior cushioning)

Solution Approach 2:

The patent uses self-assembled monolayers (SAMs) as intermediary protective layers between the plasma etching process and the dielectric material. These intermediaries enable precise etching of narrow features while shielding the dielectric from harmful etching effects, thus resolving the contradiction between dimensional accuracy and damage prevention.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach reduces defects and damage in metal structures and dielectric layers, enabling efficient bottom-up filling of narrow features with minimal voids and etching-induced damage, thereby improving the reliability and efficiency of semiconductor metallization processes.

Implementation Method 1

Applying a self-assembled monolayer selectively on the exposed metal surface

Methodology Applied
Scientific EffectSelf-assembly: Self-Assembly

Implementation Method 2

Growing a metal on the self-assembled monolayer so as to fill the at least one through-hole

Methodology Applied
Scientific EffectElectroless deposition: Electroplating

Data Source

PatentEP3029724B1Metallization method for semiconductor structures
Publication Date: 2017.06.07 INTERUNIVERSITAIR MICRO ELECTRONICS CENT (IMEC VZW)
  • EP3029724B1 patent drawingFigure 1~6
  • EP3029724B1 patent drawingFigure 7~12
  • EP3029724B1 patent drawingFigure 13~18

AI summary

A method for fabricating a semiconductor device, comprising: a. Providing a structure comprising a first sacrificial layer (2) comprising at least one through-hole exposing a metal (4) surface and optionally an oxide (5) surface, b. Applying a self-assembled monolayer (10) selectively on the exposed metal (4) surface and/or on the oxide (5) surface, c. Growing a metal (9) on the self-assembled monolayer (10) and on the exposed metal (4) surface if no self-assembled monolayer (10) is present thereon, so as to fill the at least one through-hole, thereby forming at least one metal (9) structure, d. Replacing the first sacrificial layer (2) by a replacement dielectric layer (11) having a dielectric constant of at most 3.9.