Battery Separator Coating With Metastable Aluminum Hydroxide

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Solution Overview

Problem

The flame retardant properties of lithium secondary battery separators are non-uniform even when represented by the same chemical formula, leading to inconsistent performance and safety issues.

Innovation Solution

A separator for secondary batteries is developed using a flame retardant inorganic material that exists in both stable and metastable forms, with at least 2 wt% of the metastable form, specifically aluminum hydroxide in the form of gibbsite and polymorphs like bayerite, doyleite, and nordstrandite, ensuring consistent flame retardant properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a flame retardant inorganic material is used in a separator, then flame retardant properties are improved, but the properties become non-uniform due to polymorph variations

Engineering Contradiction:
Improveflame retardant property uniformityVSAvoidpolymorph composition consistency
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent applies parameter changes by controlling the crystal structure parameters of aluminum hydroxide, specifically maintaining the metastable polymorph form (bayerite, doyleite, or nordstrandite) with specific lattice parameters and interlayer distances that differ from the stable gibbsite form. This parameter control ensures uniform flame retardant properties by preventing transformation to the stable but less effective polymorph form during storage and processing.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent utilizes phase transition principles by deliberately maintaining the flame retardant inorganic material in a metastable phase rather than allowing it to transform to the stable phase. The metastable polymorph form exhibits superior flame retardant performance, and the patent employs processing conditions and additives that kinetically stabilize this metastable phase, preventing unwanted phase transitions that would compromise performance uniformity.

Inventive Principle:
Principle #36Phase transitions

2Object-affected harmful factors

If heat-absorbing inorganic particles are added to enhance flame retardancy, then safety at high temperature is improved, but the complexity of separator composition increases

Engineering Contradiction:
Improvehigh temperature safetyVSAvoidseparator composition complexity
Core Design Contradiction:
Object-affected harmful factorsVSDevice complexity

Solution Approach 1:

The patent applies universality by selecting aluminum hydroxide as a multi-functional material that simultaneously provides flame retardancy through its decomposition reaction, heat absorption through endothermic decomposition, and physical barrier formation. This single material performs multiple safety functions, reducing the need for additional separate additives and simplifying the overall separator composition despite the enhanced safety requirements.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution ensures that the flame retardant properties are consistently exhibited, enhancing the safety and performance of lithium secondary batteries by maintaining stability and effectiveness even at elevated temperatures.

Implementation Method 1

A flame retardant separator for secondary batteries... comprising a metal hydroxide... which absorbs heat at a certain temperature

Methodology Applied
Scientific EffectEndothermic reaction: Endothermic Reaction

Implementation Method 2

the flame retardant inorganic material which can exist in a stable form and a metastable form... the separator always comprises the flame retardant inorganic material in the metastable form

Methodology Applied
Scientific EffectPhase transition: Phase Change

Data Source

PatentEP3667770B1Nonflammable secondary battery separator and corresponding secondary battery
Publication Date: 2025.04.30 LG ENERGY SOLUTION LTD
  • EP3667770B1 patent drawingFigure 1
  • EP3667770B1 patent drawingFigure 2
  • EP3667770B1 patent drawingFigure 3

AI summary

Disclosed herein is a flame retardant separator for secondary batteries, and more particularly, a flame retardant separator for secondary batteries comprising or coated with a metal hydroxide having a low Gibbs free energy among polymorphs of a metal hydroxide used as an inorganic flame retardant.