Shear Thinning Calibration Fluids for Rheometer Eccentricity Correction

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Solution Overview

Problem

Current calibration methods for rheometers, particularly at lower shear rates, are inadequate for accurately measuring the rheological properties of complex wellbore fluids due to the use of Newtonian fluids, which do not account for eccentricity and can lead to incorrect drilling parameters, inefficient operations, and subterranean formation damage.

Innovation Solution

The use of shear thinning calibration fluids that provide known shear stress profiles over a range of shear stresses or shear rates, allowing for accurate calibration of rheometers at both high and low shear rates, including eccentricity corrections, using a combination of Newtonian and shear thinning fluids to ensure precise measurements.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If Newtonian fluids are used for calibration, then the calibration process is simple, but the measurement precision at lower shear rates is inadequate due to failure to account for eccentricity

Engineering Contradiction:
Improvecalibration process simplicityVSAvoidrheological measurement precision
Core Design Contradiction:
Ease of manufactureVSMeasurement precision

Solution Approach 1:

The calibration process is segmented into two distinct parts: first calibrating with a Newtonian fluid to establish baseline torque measurements, then calibrating with a shear-thinning fluid to account for eccentricity effects. This segmentation allows each fluid type to serve its specific calibration purpose without compromising overall measurement precision.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The calibration approach uses a composite strategy combining two different fluid types (Newtonian and shear-thinning) rather than relying on a single fluid. This composite calibration method leverages the advantages of both fluid types: the simplicity of Newtonian fluid calibration and the eccentricity-correction capability of shear-thinning fluid calibration.

Inventive Principle:
Principle #40Composite materials

2Measurement precision

If shear thinning calibration fluids are used, then measurement precision and eccentricity correction are improved, but the calibration process complexity increases

Engineering Contradiction:
Improverheological measurement precisionVSAvoidcalibration process complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The Newtonian fluid calibration is performed as a preliminary step before the shear-thinning fluid calibration. This preliminary action establishes the baseline torque measurements and simplifies the subsequent shear-thinning fluid calibration by providing reference data for comparison.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The Newtonian fluid acts as an intermediary that facilitates the shear-thinning fluid calibration process. By first establishing accurate torque measurements with the Newtonian fluid, the system creates a reference framework that makes the more complex shear-thinning fluid calibration more manageable and interpretable.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Ease of operation

If single-fluid calibration methods are used, then the calibration process is straightforward, but the adaptability to different shear rates and eccentricity conditions is limited

Engineering Contradiction:
Improvecalibration operation simplicityVSAvoidcalibration adaptability to shear rates
Core Design Contradiction:
Ease of operationVSAdaptability or versatility

Solution Approach 1:

The two-fluid calibration approach creates a universal calibration system that can handle multiple calibration needs: Newtonian fluid calibration addresses high shear rate conditions and provides baseline torque data, while shear-thinning fluid calibration addresses low shear rate conditions and eccentricity correction. This multi-functional calibration system adapts to different operational requirements.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables accurate calibration of rheometers, ensuring correct drilling parameters and preventing formation damage by accounting for eccentricity and varying shear rates, thereby improving drilling efficiency and wellbore integrity.

Implementation Method 1

shear thinning calibration fluids that provide known shear stress profiles over a range of shear stresses or shear rates

Methodology Applied
Scientific EffectShear thinning: Shear Thinning

Data Source

PatentUS10184871B2Shear thinning calibration fluids for rheometers and related methods
Publication Date: 2019.01.22 HALLIBURTON ENERGY SERVICES INC
  • US10184871B2 patent drawing
  • US10184871B2 patent drawing
  • US10184871B2 patent drawing

AI summary

Shear thinning fluids may be useful as calibration fluids for calibrating rheometers with bob/rotor eccentricity and at lower shear rates, which may be particularly useful for calibrating rheometers at well sites that are used for measuring the rheological properties of complex fluids (e.g., wellbore fluids like drilling fluids, cementing fluids, fracturing fluids, completion fluids, and workover fluids). Additionally, high shear rate calibrations may also be performed with shear thinning calibration fluids. Newtonian fluids may be used for high shear rate calibrations in alternate of or in addition to the shear thinning calibration fluid.