Amplifying Sheared DNA Fragments via Hairpin Adapters

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Solution Overview

Problem

Current methods for amplifying sheared DNA fragments from biofluid samples, such as those found in cancer diagnostics, are costly and require complex data analysis, with a need for more unbiased genome-wide views and reliable amplification of nuclease-sheared nucleic acids.

Innovation Solution

A method involving dephosphorylation, digestion with sequence-specific tools, ligation to hairpin looped adapters, removal of incompletely ligated products, and amplification using primers hybridizing to the adapters, which can be performed in a single buffer system and is applicable to degraded DNA, including ctDNA and methylated DNA.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If whole genome sequencing of circulating free DNA is performed, then a comprehensive view of the tumor profile is achieved, but the cost and data analysis complexity increase significantly

Engineering Contradiction:
Improvecomprehensive view of tumor profileVSAvoiddata analysis complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent extracts and enriches only the mutation-bearing DNA sequences from the complex circulating free DNA sample using normalization techniques. This selective extraction approach allows comprehensive tumor profiling without requiring full whole genome sequencing, thereby reducing data analysis complexity while maintaining measurement precision for cancer detection.

Inventive Principle:
Principle #2Taking out (Extraction)

2Reliability

If conventional amplification methods are used for sheared DNA fragments, then amplification is achieved, but the methods are costly and require complex procedures

Engineering Contradiction:
Improveamplification reliabilityVSAvoidprocedure complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent merges multiple steps including dephosphorylation, restriction enzyme digestion, adapter ligation, and amplification into a single integrated workflow that can be performed in one reaction vessel. This consolidation reduces procedure complexity while maintaining amplification reliability for sheared DNA fragments from biofluid samples.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent develops a universal amplification method that works for various types of degraded DNA including ctDNA, cfDNA, and methylated DNA using the same set of reagents and conditions. This multi-functional approach eliminates the need for separate protocols for different DNA types, reducing overall procedure complexity while ensuring reliable amplification across all sample types.

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Quantity of substance

If mutation-bearing sequences are enriched, then sequencing cost is reduced, but the enrichment process must be reliable for degraded DNA

Engineering Contradiction:
Improvesequencing costVSAvoidenrichment reliability for degraded DNA
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent performs preliminary dephosphorylation and restriction enzyme digestion steps before adapter ligation and amplification. This preliminary processing of degraded DNA fragments ensures that the subsequent enrichment and sequencing processes work effectively on the prepared samples, maintaining enrichment reliability while reducing sequencing costs by pre-processing the complex DNA mixtures.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables reliable amplification of sheared DNA fragments, reducing sample complexity and facilitating cost-effective sequencing by enriching mutation-bearing sequences, thereby enhancing the detection and prognosis of cancer.

Implementation Method 1

dephosphorylating the sheared DNA in the sample

Methodology Applied
Scientific EffectDephosphorylation: Hydrolysis

Implementation Method 2

digesting the resulting DNA using at least one sequence specific DNA cutting tool

Methodology Applied
Scientific EffectRestriction enzyme digestion: Enzyme

Implementation Method 3

ligating the digested nucleotide sequences to hairpin looped adapters

Methodology Applied
Scientific EffectLigation: Chemical Bonding

Implementation Method 4

removing incompletely ligated products

Methodology Applied
Scientific EffectExonuclease digestion: Enzyme

Implementation Method 5

amplifying the resulting nucleotide sequences using primers hybridizing to the adapters

Methodology Applied
Scientific EffectPCR amplification: Enzyme

Data Source

PatentEP3778918B1Means and methods for amplifying nucleotide sequences
Publication Date: 2022.03.09 VLAAMS INTERUNIVERSITAIR INST VOOR BIOTECHNOLOGIE VZW
  • EP3778918B1 patent drawingFigure 1
  • EP3778918B1 patent drawingFigure 2
  • EP3778918B1 patent drawingFigure 3~4

AI summary

The present invention provides methods and kits for preparing a collection of degraded DNA fragments isolated from a biofluid sample of an individual. The prepared collection of nucleic acid sequences can be used in a diagnostic method such as for example detection and/or prognosis of cancer.