Si-QAC Antimicrobial Coating Adhesion on Low Hydroxyl Surfaces

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Solution Overview

Problem

Existing antimicrobial coatings based on quaternary ammonium silicone compounds (Si-QACs) face challenges in achieving effective binding and durability on surfaces with low hydroxyl group density, leading to poor antimicrobial efficacy and variability across different materials, particularly in in-situ cleaning and disinfection applications.

Innovation Solution

A two-step process involving the application of Si-QAC followed by a curing agent, where hypochlorite acts as a crosslinker to enhance adhesion and antimicrobial properties, and optionally incorporating tannic acid as a crosslinker to increase Si-QAC concentration, is used to create a stable and effective antimicrobial film on various surfaces.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If Si-QAC is applied directly to surfaces with low hydroxyl group density, then the application process is simple, but the binding strength and durability of the coating is poor

Engineering Contradiction:
Improveapplication process simplicityVSAvoidcoating binding strength
Core Design Contradiction:
Ease of manufactureVSStrength

Solution Approach 1:

The patent introduces a silane coupling agent as an intermediary substance between the Si-QAC and the surface. This coupling agent contains both hydrolyzable alkoxy groups that react with surface hydroxyl groups and reactive functional groups that bond with the Si-QAC, thereby mediating the interaction and enabling strong binding even on surfaces with low hydroxyl group density

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent modifies the chemical parameters of the coating system by introducing silane coupling agents with different alkoxy groups (methoxy, ethoxy, propoxy) and varying the molecular structure of the coupling agent. This allows optimization of the reaction conditions and binding strength for different surface types, including those with low hydroxyl group density

Inventive Principle:
Principle #35Parameter changes

2Reliability

If Si-QAC concentration at the surface is increased to improve antimicrobial efficacy, then the antimicrobial effectiveness improves, but the cost and complexity of the application process increases

Engineering Contradiction:
Improveantimicrobial effectivenessVSAvoidapplication process complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent applies the silane coupling agent to the surface first, allowing it to hydrolyze and form a reactive layer before applying the Si-QAC. This preliminary action prepares the surface to maximize Si-QAC binding efficiency, ensuring high antimicrobial effectiveness without requiring excessive Si-QAC concentration

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent creates a composite coating system combining the silane coupling agent and Si-QAC in a coordinated manner. The coupling agent forms a molecular bridge that concentrates and stabilizes the Si-QAC at the surface, creating a composite structure that enhances antimicrobial efficacy while maintaining application simplicity

Inventive Principle:
Principle #40Composite materials

3Device complexity

If traditional migrating disinfectants are used, then the mechanism of action is simple (leaching/diffusion), but the effectiveness is lost over time and resistant strains develop

Engineering Contradiction:
Improvemechanism of action simplicityVSAvoiddisinfectant effectiveness duration
Core Design Contradiction:
Device complexityVSDuration of action of stationary object

Solution Approach 1:

The patent segments the disinfectant system into two functional parts: a stationary silane-based coating that provides long-term structural stability and binding, and an active Si-QAC component that delivers antimicrobial function. This segmentation allows the active component to remain fixed on the surface rather than migrating, preventing resistance development while maintaining simplicity in the overall disinfection mechanism

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method significantly enhances the antimicrobial efficacy and durability of Si-QAC coatings, achieving high microbial load reduction and maintaining effectiveness even after chemical washes and thermal stress, making it suitable for long-term protection of indoor hard surfaces.

Implementation Method 1

the silane base creates the permanent covalent bond to both other molecules and the surface itself

Methodology Applied
Scientific EffectHydrolysis: Hydrolysis

Implementation Method 2

the silane base creates the permanent covalent bond to both other molecules and the surface itself

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 3

on attraction of bacteria to the surface, due to the positively charged nitrogen which draws the microorganisms towards the surface by ionic interaction

Methodology Applied
Scientific EffectIonic interaction: Ion Repulsion/Attraction

Implementation Method 4

on the mechanical kill, as the positively charged nitrogen pulls the microorganism down, the long carbon chain pierces the cells wall thereby altering its ability to properly function

Methodology Applied
Scientific EffectMechanical force: Mechanical Force

Implementation Method 5

If the cell happens to survive this disruption, the nitrogen applies the positive charge which finally neutralizes the microorganism

Methodology Applied
Scientific EffectElectrostatic interaction: Electrostatics

Implementation Method 6

Alkoxysilanes are known as coupling agents that can form Si-O bonds with hydroxyl groups

Methodology Applied
Scientific EffectChemical bonding: Chemical Bonding

Data Source

PatentEP4144217A1Antimicrobial composition for hard surfaces
Publication Date: 2023.03.08 VIRASCHUTZ EUROPE SRL
  • EP4144217A1 patent drawingFigure 1
  • EP4144217A1 patent drawingFigure 2
  • EP4144217A1 patent drawingFigure 3

AI summary

An antimicrobial composition and a kit comprising at least one quaternary ammonium silicone compound (Si-QAC) and at least one curing agent and optionally further comprising a wetting agent and/or at least one primer and/or a cross-linker being a polyphenol containing at least two hydroxyl groups their use and a method thereof for cleaning and/or disinfecting surfaces, preferably for the long-term antimicrobial protection of hard surfaces, preferably indoor surfaces are disclosed.