Si-Sn-Al Alloy Negative Electrode for Li-Ion Batteries

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Solution Overview

Problem

Lithium-ion secondary batteries using Si-based negative electrode materials face challenges with phase transition from amorphous to crystalline state, leading to volume changes and reduced cycle life, which compromises capacity and durability.

Innovation Solution

A negative electrode active material comprising an alloy with Si in the range of 12% to 100% by mass, Sn from 16% to 45% by mass, Al from 18% to 43% by mass, and minimal impurities, which suppresses phase transition and enhances cycle life and capacity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If Si-based negative electrode material is used to achieve high capacity, then discharge capacity is improved, but phase transition from amorphous to crystalline state occurs causing volume change and reduced cycle life

Engineering Contradiction:
Improvedischarge capacityVSAvoidcycle life
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The invention changes the compositional parameters by introducing specific ratios of Sn and Al elements to Si, creating an amorphous alloy system where the specific composition range (Si: 12-100%, Sn: 16-45%, Al: 18-43%) prevents crystalline phase formation during cycling, thereby maintaining structural stability and improving cycle life while preserving high capacity

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a composite amorphous alloy material combining Si, Sn, and Al elements in specific proportions. This composite structure leverages the beneficial properties of each element: Si provides high capacity, while Sn and Al suppress phase transition and maintain amorphous structure stability, resulting in a material that achieves both high discharge capacity and excellent cycle durability

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If Si content is increased to enhance capacity, then energy density is improved, but volume change during alloying with Li increases reducing electrode durability

Engineering Contradiction:
Improveenergy densityVSAvoidvolume stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The invention optimizes the compositional parameters by establishing specific content ranges for Si, Sn, and Al elements. By controlling Si content within 12-100% while simultaneously introducing Sn (16-45%) and Al (18-43%), the material achieves high energy density while the Sn and Al components constrain volume expansion and maintain compositional stability during Li alloying cycles

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The Si-Sn-Al-based alloy maintains high capacity and cycle durability, with discharge capacity retention of 92% at the 50th cycle and 55% at the 100th cycle, outperforming conventional materials.

Implementation Method 1

when Si and Li are alloyed, transition from an amorphous state to a crystalline state is generated. As the result, a large volume change occurs, and there is such a problem that a cycle life of the electrode decreases

Methodology Applied
Scientific EffectPhase transition suppression: Phase Change

Data Source

PatentEP2717355B1Negative electrode active material for electrical devices
Publication Date: 2016.06.22 NISSAN MOTOR CO LTD
  • EP2717355B1 patent drawingFigure 1
  • EP2717355B1 patent drawingFigure 2
  • EP2717355B1 patent drawingFigure 3

AI summary

The negative electrode active material for an electric device of the present invention has an alloy containing Si in a range from 12% by mass or more to less than 100% by mass, Sn in a range from more than 0% by mass to 45% by mass or less, Al in a range from more than 0% by mass to 43% by mass or less, and indispensable impurities as remains. The negative electrode active material can be obtained, for example, using a multiple DC magnetron sputtering apparatus with Si, Sn and Al as targets. Electric devices to which the negative electrode active material of the present invention is applied have an improved cycle life and are excellent in the capacity and cycle durability.