SiC Boule Growth Using Polymer-Derived Volumetric Shapes

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Solution Overview

Problem

There is a long-standing need for cost-effective methods to produce high-quality single crystal SiC boules for electronic components, as existing methods are inefficient and expensive.

Innovation Solution

The development of volumetric shapes made from polymer-derived SiC using a binder, which are then used in vapor deposition processes to form SiC boules, allowing for controlled flux formation and improved boule quality.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If conventional methods are used to produce SiC boules, then the process is established and reproducible, but the manufacturing cost is high and efficiency is low

Engineering Contradiction:
Improvemanufacturing costVSAvoidproduction efficiency
Core Design Contradiction:
Ease of manufactureVSProductivity

Solution Approach 1:

The invention changes the physical-chemical parameters of the starting material by using polymer-derived SiC granules with specific characteristics (particle size distribution, surface area, reactivity) instead of conventional SiC sources. This parameter change enables more efficient vapor deposition while maintaining process control, thereby reducing manufacturing cost and improving productivity simultaneously

Inventive Principle:
Principle #35Parameter changes

2Manufacturing precision

If polymer-derived SiC granules are used as starting material, then flux formation is controlled and boule quality is improved, but the process complexity increases

Engineering Contradiction:
Improveboule qualityVSAvoidprocess complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The polymer-derived SiC granules are prepared in advance with specific properties (particle size, surface area, reactivity) that pre-determine the flux formation characteristics during vapor deposition. This preliminary preparation of the starting material with optimized properties simplifies the actual deposition process while ensuring high boule quality, as the material is pre-conditioned to react predictably

Inventive Principle:
Principle #10Preliminary action

3Volume of stationary object

If vapor deposition is used to grow large boules, then boule size is increased, but the growth time and energy consumption increase

Engineering Contradiction:
Improveboule sizeVSAvoidgrowth time
Core Design Contradiction:
Volume of stationary objectVSLoss of time

Solution Approach 1:

The vapor deposition process using polymer-derived SiC granules maintains continuous and stable flux formation throughout the growth cycle, preventing interruptions or slowdowns. The high reactivity and controlled sublimation of the polymer-derived material ensure consistent material supply to the growing boule, enabling faster growth rates and reducing total growth time while achieving large boule sizes

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method enables the production of high-quality SiC boules with consistent flux formation, increased boule size, and reduced defects, leading to improved electronic component performance and reduced manufacturing costs.

Implementation Method 1

a binder, wherein the binder binds the SiC granules

Methodology Applied
Scientific EffectAdhesion: Adhesive

Implementation Method 2

Silicon carbide does not generally have a liquid phase, instead it sublimes, under vacuum, at temperatures above about 1,700° C.

Methodology Applied
Scientific EffectSublimation: Sublimation

Implementation Method 3

a solid or liquid starting material is transformed into a gas or vapor state, and then the gas or vapor is deposited to form, e.g., grow, a solid material

Methodology Applied
Scientific EffectVapor deposition: Physical Vapour Deposition

Data Source

PatentUS12330948B2SiC volumetric shapes and methods of forming boules
Publication Date: 2025.06.17 PALLIDUS INC
  • US12330948B2 patent drawing
  • US12330948B2 patent drawing
  • US12330948B2 patent drawing

AI summary

Volumetric shapes of SiC starting materials for boule growth. Methods of controlling vapor deposition growth of SiC boules, and providing directional flux. Methods of increase the number of wafers, the number of electronic components and the number of operable devices from a single boule growth cycle.