SiC Crystal Growth Clogging Prediction via Pressure Monitoring

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Solution Overview

Problem

The challenge in growing long silicon carbide (SiC) single crystals is the accumulation of solid deposits within the manufacturing apparatus, which clogs gas flow passages and disrupts the continuous supply of SiC source gas, making it difficult to predict and prevent clogging.

Innovation Solution

A SiC single crystal manufacturing apparatus equipped with a pressure sensor and a computing device that uses machine learning to predict clogging time based on gas pressure measurements and a learning model created from simulations and experimental data, allowing for the anticipation and management of clogging events.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Length of moving object

If gas growth method is used to grow long SiC single crystal, then the crystal length can be increased, but solid deposit accumulates and clogs gas flow passages interrupting gas supply

Engineering Contradiction:
ImproveSiC single crystal lengthVSAvoidgas supply continuity
Core Design Contradiction:
Length of moving objectVSReliability

Solution Approach 1:

The system performs preliminary action by predicting clogging time before actual clogging occurs. The prediction unit uses machine learning models to forecast when solid deposits will clog the gas introduction pipe, allowing operators to take preventive measures such as cleaning or maintenance before the clogging actually happens, thus maintaining gas supply continuity while enabling long crystal growth

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The system implements feedback by continuously monitoring gas pressure and feeding this information to the prediction unit. The pressure sensor provides real-time data about gas flow conditions, which the machine learning model uses to update clogging time predictions. This closed-loop feedback system allows dynamic adjustment and early warning of potential clogging issues

Inventive Principle:
Principle #23Feedback

2Reliability

If solid deposit accumulates in gas flow passage, then clogging occurs disrupting growth conditions, but continuous monitoring and prediction systems increase device complexity

Engineering Contradiction:
Improvegrowth condition stabilityVSAvoidmonitoring system complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The system replaces complex mechanical monitoring approaches with a computational intelligence-based solution. Instead of using multiple physical sensors and mechanical detection devices, the invention uses machine learning algorithms that process simple pressure data to predict clogging. This substitution of mechanical/physical monitoring systems with computational models reduces overall device complexity while maintaining high reliability

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The machine learning prediction unit acts as an intermediary between the simple pressure sensor data and the complex phenomenon of solid deposit accumulation. Rather than directly monitoring difficult-to-measure parameters like deposit thickness or composition, the system uses pressure as an intermediary parameter that the ML model correlates with clogging risk, simplifying the monitoring requirement

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables the accurate prediction of clogging times, reducing the risk of apparatus failure and allowing for the continuous growth of long SiC single crystals by identifying potential clogging states through observable gas pressure parameters.

Implementation Method 1

a gas pressure of the supply gas measured by a pressure sensor

Methodology Applied
Scientific EffectPressure measurement:

Implementation Method 2

the heating device is configured to heat and decompose the SiC raw material gas

Methodology Applied
Scientific EffectThermal decomposition: Pyrolysis

Implementation Method 3

a learning model created by machine learning using data calculated from results of simulations of growing the SiC single crystal and results of experiments of growing the silicon carbide single crystal

Methodology Applied
Scientific EffectMachine learning prediction:

Data Source

PatentUS20250092569A1Silicon carbide single crystal manufacturing apparatus, computing device, and manufacturing method of silicon carbide single crystal
Publication Date: 2025.03.20 DENSO CORP
  • US20250092569A1 patent drawing
  • US20250092569A1 patent drawing
  • US20250092569A1 patent drawing

AI summary

A silicon carbide single crystal manufacturing apparatus includes a pressure sensor and a computing device. The pressure sensor is configured to measure a gas pressure of a supply gas containing a silicon carbide raw material gas and introduced into a crucible through a gas introducing pipe. The computing device is configured to perform a prediction of a clogging time, which is a time until the gas introduction pipe is clogged with a solid deposit, based on the gas pressure measured by the pressure sensor a learning model created by machine learning using data calculated from results of simulations of growing the silicon carbide single crystal and results of experiments of growing the silicon carbide single crystal.