SiC Substrate Heat Treatment for BPD and Step Bunching Reduction

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Solution Overview

Problem

SiC substrates and epitaxial substrates suffer from crystal defects such as basal plane dislocation (BPD) and step bunching, which adversely affect the performance and reliability of SiC semiconductor devices.

Innovation Solution

A method involving a heat treatment process with multiple steps to remove strained layers, macro step bunching, and reduce basal plane dislocations, including etching and crystal growth in controlled environments with temperature gradients and specific vapor pressures to produce high-quality SiC substrates.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional SiC substrate production methods are used, then manufacturing simplicity is maintained, but crystal defects such as basal plane dislocation and step bunching occur, reducing device reliability

Engineering Contradiction:
Improvedevice reliabilityVSAvoidproduction process complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The heat treatment process is divided into multiple sequential steps: initial heat treatment to remove strained layers, followed by epitaxial growth to form a growth layer, then additional heat treatment to remove step bunching, and finally conversion heat treatment to transform basal plane dislocations into threading edge dislocations. Each step targets specific defects independently, achieving comprehensive defect reduction through process segmentation.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The method performs preliminary heat treatment and epitaxial growth before final device fabrication to pre-remove strained layers and reduce dislocation densities. By addressing defect formation early in the process chain, the subsequent device manufacturing steps operate on a cleaner substrate, improving final device reliability without adding complexity to the core fabrication process.

Inventive Principle:
Principle #10Preliminary action

2Manufacturing precision

If heat treatment is performed to remove strained layers and reduce dislocations, then substrate quality improves, but production time and process steps increase

Engineering Contradiction:
Improvesubstrate qualityVSAvoidproduction time
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

Multiple defect removal functions are merged into a single integrated heat treatment process. The process combines strained layer removal, step bunching elimination, and basal plane dislocation conversion into one continuous heat treatment sequence with epitaxial growth, eliminating the need for separate treatment steps and reducing overall production time while maintaining high substrate quality.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The heat treatment process utilizes precise control of temperature parameters and atmospheric conditions to achieve multiple defect removal objectives simultaneously. By optimizing temperature gradients, exposure times, and chemical environment parameters, the process efficiently removes different types of defects in a coordinated manner, improving substrate quality without proportionally increasing processing time.

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If step bunching is present on the SiC substrate surface, then substrate production remains simple, but defect formation occurs during epitaxial growth, reducing epitaxial layer quality

Engineering Contradiction:
Improveepitaxial layer qualityVSAvoidsubstrate preparation ease
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The method performs preliminary heat treatment before epitaxial growth to remove step bunching from the substrate surface. By eliminating step bunching in advance, the subsequent epitaxial growth proceeds on a flat, uniform surface, preventing defect formation in the epitaxial layer and ensuring high layer quality without complicating the substrate preparation process.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The heat treatment process acts as an intermediary step between substrate production and epitaxial growth. This intermediate treatment removes step bunching and prepares the substrate surface, serving as a bridge that connects simple substrate manufacturing with high-quality epitaxial layer formation, ensuring defect-free growth while maintaining ease of manufacture.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method effectively reduces defects in SiC substrates, enabling the production of high-quality SiC epitaxial substrates and ingots with improved performance and reliability.

Implementation Method 1

a heat treatment step of heat-treating a SiC base substrate

Methodology Applied
Scientific EffectHeat treatment: Heat Treatment

Implementation Method 2

Basal plane dislocation reduction step of forming a growth layer in which basal plane dislocation is reduced, on the SiC base substrate

Methodology Applied
Scientific EffectCrystal growth: Crystallisation

Data Source

PatentUS12421624B2SiC substrate, SiC epitaxial substrate, SiC ingot and production methods thereof
Publication Date: 2025.09.23 TOYOTA TSUSHO CORP
  • US12421624B2 patent drawing
  • US12421624B2 patent drawing
  • US12421624B2 patent drawing

AI summary

The present invention addresses the problem of providing a novel technology which enables the achievement of a high-quality SiC substrate, a high-quality SiC epitaxial substrate, and a high-quality SiC ingot. The present invention is a method for producing an SiC substrate 11, said method comprising a heat treatment step S1 for heat treating an SiC base substrate 10, said heat treatment step S1 comprising two or more steps among the steps (a), (b) and (c) described below. (a) a strained layer removal step S11 for removing a strained layer 101 of the SiC base substrate 10. (b) a bunching removal step S12 for removing macro-step bunching (MSB) on the SiC base substrate 10. (c) a basal plane dislocation reduction step S13 for forming a growth layer 105, in which basal plane dislocations (BPD) are reduced, on the SiC base substrate 10.