SiGe Selective Etching Solution for Stable Semiconductor Manufacturing

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Solution Overview

Problem

Existing etching solutions for SiGe compounds in semiconductor manufacturing often result in etching stops and unintentional etching of Si layers, leading to unstable transistor characteristics and reduced yield, due to the complexity and inefficiency of current methods.

Innovation Solution

An etching solution comprising hydrofluoric acid, nitric acid, and water, with specific concentration ranges (0.002-1.0% for hydrofluoric acid, 10-55% for nitric acid, and up to 40% for water), which selectively etches SiGe compounds while preventing etching stops and improving etching rates.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional fluorine nitric acid solution is used for selective etching of SiGe layer, then high etching ratio for SiGe is achieved, but etching stops occur after prolonged etching time

Engineering Contradiction:
Improveetching selectivityVSAvoidetching duration
Core Design Contradiction:
Manufacturing precisionVSDuration of action of stationary object

Solution Approach 1:

The patent modifies the chemical composition parameters of the etching solution by adding acetic acid and adjusting the concentrations of hydrofluoric acid, nitric acid, and water. This parameter change enables the solution to maintain stable etching performance over extended periods without etching stops, resolving the contradiction between selectivity and duration.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If conventional etching solution is used for prolonged etching, then complete SiGe removal is achieved, but unintentional Si layer etching occurs

Engineering Contradiction:
Improveetching efficiencyVSAvoidetching control
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent optimizes the concentration parameters of hydrofluoric acid (0.002-1.0%), nitric acid (10-55%), and acetic acid (5-40%) to achieve a balanced etching rate. This parameter optimization allows prolonged etching to remove complete SiGe layers while maintaining control and preventing unintentional Si layer etching.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If multiple etching steps with water washing are implemented, then etching stop problem is solved, but manufacturing complexity and cost increase

Engineering Contradiction:
Improveetching stabilityVSAvoidprocess complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent extracts the water washing steps from the etching process by formulating a single etching solution that inherently prevents etching stops through the addition of acetic acid. This eliminates the need for repeated immersion and washing operations, reducing process complexity while maintaining reliability.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent combines multiple functions into a single etching solution formulation that provides both selective etching capability and prevention of etching stops. The merged solution eliminates the need for separate etching and washing steps, simplifying the overall process while maintaining stability.

Inventive Principle:
Principle #5Merging (Combining)

4Loss of time

If conventional etching solution is used, then short etching time is required, but etching stops occur and yield deteriorates

Engineering Contradiction:
Improveetching timeVSAvoidyield
Core Design Contradiction:
Loss of timeVSReliability

Solution Approach 1:

The patent changes the chemical parameters of the etching solution by incorporating acetic acid and optimizing the ratios of other components. This enables prolonged etching times to be used effectively, improving yield by allowing complete SiGe removal without etching stops while maintaining reasonable process efficiency.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution enables stable and selective etching of SiGe compounds, suppressing etching stops and improving etching uniformity, thereby enhancing manufacturing efficiency and reducing costs by allowing longer etching times without complex process steps.

Implementation Method 1

an etching solution containing hydrofluoric acid (DHF) and nitric acid has a high etching ratio for a SiGe compound with respect to Si, SiO2, and the like

Methodology Applied
Scientific EffectChemical etching: Chemical Bonding

Implementation Method 2

an etching solution containing hydrofluoric acid (DHF) and nitric acid has a high etching ratio for a SiGe compound

Methodology Applied
Scientific EffectOxidation: Oxidation

Data Source

PatentUS11518937B2Etching solution and method for manufacturing semiconductor element
Publication Date: 2022.12.06 TOKYO OHKA KOGYO CO LTD

AI summary

An etching solution for selectively performing an etching process on a compound represented by General Formula Si1-xGex, in which x is more than 0 and less than 1, with respect to Si, Ge, and oxides thereof, the etching solution including hydrofluoric acid, nitric acid, and water, in which a content ratio of the hydrofluoric acid in the entire etching solution is 0.002% by mass or more and 1.0% by mass or less, a content ratio of the nitric acid in the entire etching solution is 10% by mass or more, and a content ratio of the water in the entire etching solution is 40% by mass or less.