Multi-layer Silage Film with Density-Graded Ethylene Copolymers

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Solution Overview

Problem

Polyethylene-based silage films incorporating polyisobutylene (PIB) face challenges such as process control difficulties due to PIB's liquid state at ambient temperatures, capital expenditures for liquid dosage systems, and migration issues at elevated temperatures, leading to film blocking and equipment jamming, necessitating a PIB-free or low-PIB film with maintained toughness and cling properties.

Innovation Solution

A multi-layer film with at least three layers, featuring two outer layers and a core layer, where the core layer comprises an ethylene copolymer with 1-octene and specific density ranges, and the outer layers include ethylene copolymers with densities between 0.850 and 0.890 g/cm³, enhancing cling properties and reducing component migration at elevated temperatures.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If polyisobutylene is added to improve cling properties, then cling properties are improved, but process control difficulties and capital expenditures for liquid dosage systems occur

Engineering Contradiction:
Improvecling propertiesVSAvoidliquid dosage systems
Core Design Contradiction:
Ease of operationVSDevice complexity

Solution Approach 1:

The invention changes the physical state parameter of the adhesive component from liquid (PIB requiring dosage systems) to solid form (masterbatch), eliminating the need for complex liquid dosing equipment while maintaining cling properties

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses a masterbatch as an intermediary carrier to deliver the PIB adhesive component in solid form, which then melts and distributes during the extrusion process, replacing the need for direct liquid dosing systems

Inventive Principle:
Principle #24Intermediary (Mediator)

2Strength

If polyisobutylene is used to enhance film properties, then toughness and cling are improved, but migration occurs at elevated temperatures causing film blocking

Engineering Contradiction:
ImprovetoughnessVSAvoidfilm blocking
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The invention places the PIB-containing adhesive layer specifically in the inner layer of the multi-layer structure, where it performs its cling function, while outer layers use migration-resistant polymers to prevent blocking at high temperatures

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The invention creates a multi-layer composite film structure combining PIB-based adhesive layer for cling properties with migration-resistant polymer layers for thermal stability, achieving both toughness and resistance to film blocking

Inventive Principle:
Principle #40Composite materials

3Device complexity

If masterbatch comprising PIB is used instead of liquid dosing, then liquid dosage systems are eliminated, but a masterbatch compounding step must be included

Engineering Contradiction:
Improveliquid dosage systemsVSAvoidmasterbatch compounding step
Core Design Contradiction:
Device complexityVSProductivity

Solution Approach 1:

The PIB adhesive component is pre-compounded into a masterbatch form before the film extrusion process, allowing it to be readily available in a stable, solid form that can be easily fed into the extruder without requiring liquid dosing equipment during production

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The multi-layer film achieves improved cling properties and reduced component migration during storage and use at high temperatures, while eliminating the need for precise liquid dosing and masterbatch compounding, thus addressing the drawbacks of PIB-containing films.

Implementation Method 1

the core layer comprises an ethylene copolymer comprising 1-octene and having a density between > 0.910 g/cm³ and 0.915 g/cm³

Methodology Applied
Scientific EffectAdhesion: Adhesive

Implementation Method 2

such film demonstrates improved cling properties and further provides benefits in that a.o. migration of components from this film during storage and use at elevated temperatures is reduced

Methodology Applied
Scientific EffectPhysical containment: Physical Containment

Data Source

PatentEP3642033B1Silage film solutions
Publication Date: 2022.04.13 SABIC GLOBAL TECHNOLOGIES BV

AI summary

The present invention relates to a multi-layer film comprising at least three layers, with two outer layers, and one core layer, wherein: ⋅ the core layer comprises an ethylene copolymer comprising 1-octene and having a density between > 0.910 g/cm3 and 0.925 g/cm3, wherein further ⋅ the first outer layer comprises an ethylene homopolymer having a density of between > 0.915 g/cm3 and 0.930 g/cm3, wherein further ⋅ the second outer layer comprises and optional first ethylene copolymer and a second ethylene copolymer having a density of between 0.850 g/cm3 and < 0.890 g/cm3. Such film demonstrates improved cling properties and further provides benefits in that a.o. migration of components from this film during storage and use at elevated temperatures is reduced.