Organofunctional Silane Adhesion on Glass Coatings

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Solution Overview

Problem

Existing methods for coating glass substrates fail to achieve strong adhesion of organic coatings, leading to poor durability and ultraviolet protection, as conventional processes require undesirable energy treatments like flame, corona, or plasma to achieve adhesion.

Innovation Solution

A method involving the deposition of a silicon-based inorganic oxide coating on glass, followed by an organofunctional silane application, and then an organic coating, which creates a highly reactive surface for enhanced bonding, eliminating the need for energy treatments.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If conventional coating processes are used on glass substrates, then the coating can be applied, but adhesion strength is poor and energy treatments are required

Engineering Contradiction:
Improveadhesion strengthVSAvoidenergy treatment requirement
Core Design Contradiction:
StrengthVSUse of energy by moving object

Solution Approach 1:

The patent applies preliminary chemical treatments to the glass substrate surface before coating application. Specifically, it uses silane coupling agents and metal oxide primers that are applied in advance to create a chemically active surface layer that will bond strongly with the subsequent organic coating, eliminating the need for energy-intensive flame or plasma treatments at the coating stage

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent introduces intermediary layers between the glass substrate and the organic coating. These intermediaries include metal oxide primers (such as tin oxide or zinc oxide) and silane coupling agents that act as chemical mediators, forming strong bonds with both the glass substrate and the organic coating, thereby achieving strong adhesion without requiring external energy treatment

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If conventional coating processes are used on glass substrates, then the coating can be applied, but durability and ultraviolet protection are poor

Engineering Contradiction:
Improvedurability and ultraviolet protectionVSAvoidadhesion strength
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The patent employs composite coating structures consisting of multiple functional layers. The composite system includes a glass substrate, metal oxide primer layer, silane coupling agent layer, and organic coating layer. Each layer contributes specific properties: the metal oxide provides UV absorption and chemical stability, the silane provides strong chemical bonding, and the organic coating provides durability and aesthetic properties, collectively achieving both strong adhesion and enhanced durability with UV protection

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach results in significantly improved adhesion strength of organic coatings on glass containers, enhancing durability and ultraviolet protection, with adhesion strength being two to three times greater than conventional surface treatments.

Implementation Method 1

depositing a silicon-based inorganic oxide on an exterior surface of the glass

Methodology Applied
Scientific EffectDeposition: Deposition (physical)

Implementation Method 2

applying an organofunctional silane to the glass over the inorganic oxide

Methodology Applied
Scientific EffectChemical bonding: Chemical Bonding

Data Source

PatentEP2556036B1Improving adhesion of organic coatings on glass
Publication Date: 2020.07.15 OWENS BROCKWAY GLASS CONTAINER INC
  • EP2556036B1 patent drawingFigure 1~2

AI summary

Methods of manufacturing and coating glass including depositing an inorganic oxide on an exterior surface of the glass, and then applying an organofunctional silane to the glass over the inorganic oxide. The methods also may include applying an organic coating to the glass over the organofunctional silane, and curing the organic coating.