Silicon Anode Composite With Nitride Phase for Cycle Durability

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Solution Overview

Problem

Silicon compounds in negative electrode active materials for secondary batteries are prone to erosion due to side reactions, leading to capacity degradation and reduced durability.

Innovation Solution

Incorporating a silicon nitride phase dispersed in a silicon compound phase, such as silicon oxide or silicate phase, to enhance durability and improve charge and discharge cycle characteristics by mitigating stress from lithium ion expansion and contraction.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If silicon compound phase is used in negative electrode active material, then theoretical capacity density improves, but durability deteriorates due to erosion from side reactions with hydrogen fluoride

Engineering Contradiction:
Improvetheoretical capacity densityVSAvoiddurability
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent employs a composite material structure consisting of a silicon compound phase (such as silicon oxide or silicate) combined with a silicon nitride phase. The silicon nitride phase acts as a protective component that reduces erosion from hydrogen fluoride while the silicon compound phase provides high theoretical capacity density through lithium alloying. This composite approach allows simultaneous achievement of high capacity and improved durability.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The silicon nitride phase serves as an intermediary protective layer between the silicon compound phase and the corrosive hydrogen fluoride in the electrolyte. It mediates the interaction by providing chemical stability and resistance to erosion, thereby protecting the reactive silicon compound phase from degradation while allowing lithium ion transport.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Quantity of substance

If silicon compound phase is used to achieve high capacity, then charge and discharge cycle characteristics worsen due to gradual erosion and capacity deterioration

Engineering Contradiction:
ImprovecapacityVSAvoidcharge and discharge cycle characteristics
Core Design Contradiction:
Quantity of substanceVSDuration of action of moving object

Solution Approach 1:

The composite structure of silicon compound phase with dispersed silicon nitride phase provides both high capacity and improved cycle characteristics. The silicon nitride phase maintains structural integrity during charge-discharge cycles and protects against gradual erosion, enabling sustained performance over extended cycling.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The silicon nitride phase is dispersed locally within the silicon compound phase, providing targeted protection at specific locations where erosion is most likely to occur. This local reinforcement strategy maintains overall high capacity while improving durability at critical interfaces.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The silicon nitride phase effectively suppresses erosion of the silicon compound phase, resulting in improved durability and enhanced charge and discharge cycle characteristics of secondary batteries.

Implementation Method 1

use of a material containing silicon capable of being alloyed with lithium

Methodology Applied
Scientific EffectAlloying:

Implementation Method 2

a silicon nitride phase dispersed in the silicon compound phase, wherein the silicon compound phase is at least one of a silicon oxide phase and a silicate phase

Methodology Applied
Scientific EffectStress relief: Stress Relaxation

Data Source

PatentEP4379860B1Negative electrode active material for secondary batteries, and secondary battery
Publication Date: 2026.03.11 PANASONIC INTELLECTUAL PROPERTY MANAGEMENT CO LTD
  • EP4379860B1 patent drawingFigure 1
  • EP4379860B1 patent drawingFigure 2
  • EP4379860B1 patent drawingFigure 3~4

AI summary

A negative electrode active material for a secondary battery includes Si-containing particles, wherein the Si-containing particles include a silicon compound phase, a silicon phase dispersed in the silicon compound phase, and a silicon nitride phase dispersed in the silicon compound phase, and the silicon compound phase is at least one of a silicon oxide phase and a silicate phase.