Silicon-Coated Carbon Anode for Stable High-Capacity Li-Ion Batteries

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Solution Overview

Problem

Lithium secondary batteries face challenges with silicon-based anode materials that cause side reactions, contraction, and expansion, leading to reduced lifespan and stability, especially when exposed to moisture and air, necessitating a solution for high capacity and stability.

Innovation Solution

A carbon-based anode active material layer with a silicon coating, where the silicon content on the surface is controlled between 3 atom% to 25 atom% and the Si—O peak intensity ratio is between 0.05 to 1, formed using a dry deposition process to prevent gas generation and maintain conductivity, is used.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If silicon-based material is used as anode active material, then capacity is improved, but side reactions with moisture and air occur causing reduced stability

Engineering Contradiction:
ImprovecapacityVSAvoidstability
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

A carbon coating layer is introduced as an intermediary between the silicon-based active material and the external environment (moisture, air, electrolyte). This carbon layer prevents direct contact and side reactions while allowing lithium ion transport, thus maintaining high capacity benefits of silicon while improving stability and lifespan

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The anode is designed as a composite structure combining silicon-based active material particles with a carbon coating layer. This composite approach leverages the high capacity of silicon while the carbon component provides chemical stability, moisture resistance, and structural integrity during cycling

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If silicon-based material is used as anode active material, then capacity is improved, but contraction and expansion occur during charging and discharging

Engineering Contradiction:
ImprovecapacityVSAvoidstructural stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The carbon coating layer acts as a flexible shell that can accommodate the volume changes of silicon during lithiation and delithiation. This shell maintains structural integrity, prevents particle fragmentation, and ensures continuous electrical contact throughout cycling

Inventive Principle:
Principle #30Flexible shells and thin films

Solution Approach 2:

The carbon coating is applied beforehand to the silicon particles, creating a protective cushion that absorbs mechanical stress from expansion and contraction. This pre-established protective layer prevents direct mechanical failure of the silicon structure during volume changes

Inventive Principle:
Principle #11Beforehand cushioning (Prior cushioning)

3Reliability

If conventional anode active material is used, then stability is maintained, but high capacity is not achieved

Engineering Contradiction:
ImprovestabilityVSAvoidcapacity
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The invention creates a composite anode structure where silicon-based material (providing high capacity) is combined with carbon coating (providing stability). This composite approach allows the system to achieve both high capacity and good stability simultaneously, overcoming the limitation of conventional single-material anodes

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances capacity and energy density while reducing gas generation and anode resistance, ensuring improved stability and lifespan of the lithium secondary battery.

Implementation Method 1

formed using a dry deposition process to prevent gas generation and maintain conductivity

Methodology Applied
Scientific EffectDry deposition: Physical Vapour Deposition

Implementation Method 2

A surface content of silicon of the anode active material layer measured by an X-ray photoelectric spectroscopy (XPS)

Methodology Applied
Scientific EffectX-ray photoelectric spectroscopy: Photoelectric Effect

Data Source

PatentEP4199137B1Anode for secondary battery, method of fabricating the same and lithium secondary battery including the same
Publication Date: 2024.12.18 SK ON CO LTD
  • EP4199137B1 patent drawingFigure 1
  • EP4199137B1 patent drawingFigure 2~3
  • EP4199137B1 patent drawingFigure 4~5

AI summary

An anode active material for a secondary battery includes an anode current collector, and an anode active material layer formed on the anode current collector and including carbon-based active material particles and a silicon coating formed on surfaces of the carbon-based active material particles. A surface content of silicon of the anode active material layer measured by an X-ray photoelectric spectroscopy (XPS) is in a range from 3 atom% to 25 atom%. A peak intensity ratio defined as a ratio of a second peak intensity corresponding to a peak intensity at a binding energy in a range from 102 eV to 106 eV relative to a first peak intensity corresponding to a peak intensity at a binding energy in a range from 98 eV to 102 eV is in a range from 0.05 to 1.