Silicon Nanotube Cathode for Lithium Battery Cycle Life

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Solution Overview

Problem

Lithium secondary batteries using conventional inorganic negative-electrode active materials like silicon suffer from low cycle life and capacity retention due to volume changes during charge/discharge, leading to pulverization and loss of reversible capacity.

Innovation Solution

A nanotube-based negative-electrode active material with a thin amorphous carbon layer on its outer and/or inner sides, made from non-carbonaceous materials like silicon, germanium, or antimony, which absorbs volume changes and maintains structural integrity during cycling, enhancing cycle life and capacity retention.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If inorganic negative-electrode active material like silicon is used, then charge capacity is improved, but cycle life and capacity retention deteriorate due to volume change and pulverization

Engineering Contradiction:
Improvecharge capacityVSAvoidcycle life
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The silicon-based active material is divided into nanoscale particles (1-100 nm), which segment the material into small units that can independently accommodate volume changes during lithium insertion/extraction, preventing macroscopic pulverization and maintaining structural integrity over many cycles

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Silicon nan particles are embedded within a porous carbon matrix structure, where the carbon framework provides mechanical support and confinement space for the silicon particles, allowing the silicon to expand and contract without losing electrical contact or structural stability

Inventive Principle:
Principle #7Nested doll (Nesting)

Solution Approach 3:

A porous carbon matrix with controlled pore size and structure is used to host the silicon nanoparticles, providing pathways for lithium ion diffusion while maintaining structural flexibility to accommodate silicon volume changes during charge-discharge cycles

Inventive Principle:
Principle #31Porous materials

2Quantity of substance

If inorganic negative-electrode active material is used, then charge capacity is improved, but capacity retention deteriorates due to pulverization and aggregation

Engineering Contradiction:
Improvecharge capacityVSAvoidcapacity retention
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

A composite structure combining silicon nanoparticles with a porous carbon matrix is created, where the carbon component provides structural stability and electrical conductivity while the silicon nanoparticles provide high lithium capacity, achieving both high capacity and excellent capacity retention

Inventive Principle:
Principle #40Composite materials

3Reliability

If graphite is used as negative-electrode active material, then cycle life is improved, but charge capacity deteriorates due to low theoretical capacity

Engineering Contradiction:
Improvecycle lifeVSAvoidcharge capacity
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The active material is changed from graphite (theoretical capacity 372 mAh/g) to silicon-based materials (theoretical capacity up to 4200 mAh/g for Li4.1Si), dramatically increasing the charge capacity parameter while maintaining acceptable cycle life through the nanoscale composite structure

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The nanotube structure with a thin carbon layer effectively reduces capacity loss and maintains excellent cycle life and capacity retention, outperforming previous materials by maintaining morphology and capacity after 200 cycles.

Implementation Method 1

the inorganic negative-electrode active material such as silicon-based negative-electrode active material causes considerable volume change at intercalation/deintercalation of lithium, i.e., charge/discharge of a battery

Methodology Applied
Scientific EffectVolume change absorption:

Implementation Method 2

the nanotube structure with a thin carbon layer effectively reduces capacity loss and maintains excellent cycle life and capacity retention, outperforming previous materials by maintaining morphology and capacity after 200 cycles

Methodology Applied
Scientific EffectStructural stability maintenance:

Implementation Method 3

A battery generates electric power using material capable of electrochemical reactions in a positive- and a negative-electrode. A representative example of the battery is a lithium secondary battery which generates electrical energy by chemical potential change when lithium ions are intercalated/deintercalated in a positive- and a negative-electrode

Methodology Applied
Scientific EffectElectrochemical reactions:

Data Source

PatentEP2445040B1Cathode active material for a lithium rechargeable battery and a production method therefor
Publication Date: 2018.08.01 LG CHEM LTD
  • EP2445040B1 patent drawingFigure 1~2(a)
  • EP2445040B1 patent drawingFigure 2(b)~2(c)
  • EP2445040B1 patent drawingFigure 2(d)~2(e)

AI summary

The present invention relates to negative-electrode active material for a lithium secondary battery exhibiting excellent capacity property and cycle life property, a method of preparing the same, and a lithium secondary battery using the negative-electrode active material, wherein the negative-electrode active material for a lithium secondary battery comprises a nanotube having a tube shape defined by an outer wall with a thickness of nanoscale, the outer wall of the nanotube comprises at least one non-carbonaceous material selected from the group consisting of silicon, germanium and antimony, and an amorphous carbon layer with a thickness of 5 nm or less is formed on the outer wall of the nanotube.