Silicon Nitride Ceramic Heater for Rapid Thermal Cycling

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Solution Overview

Problem

Conventional ceramic heaters experience electrical disconnection at an early stage when subjected to ultrahigh-speed temperature raising, which is necessary for reducing emissions in combustion chambers, due to repeated thermal stress, limiting their service life.

Innovation Solution

A ceramic heater with a heat-generating element formed from silicon nitride and an electrically conductive material, having a U-shaped configuration and high fracture toughness, is integrated into an insulating ceramic substrate, and the heat-generating portion is designed to be thinner than the lead portions to enhance thermal resistance and rapid temperature rise capabilities.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If conventional ceramic heater materials are used, then heat resistance is improved, but electrical disconnection occurs at early stage under ultrahigh-speed temperature raising

Engineering Contradiction:
Improveheat resistanceVSAvoidelectrical disconnection resistance
Core Design Contradiction:
TemperatureVSReliability

Solution Approach 1:

The heat-generating element is formed as a composite material containing silicon nitride ceramic particles (3-10 μm diameter, 40-70 wt%) dispersed in a binder material. This composite structure achieves both high heat resistance from the silicon nitride ceramic and high fracture toughness (4.3 MPa·m^0.5 or more) to prevent electrical disconnection under repeated thermal stress during ultrahigh-speed temperature raising.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention optimizes specific parameters including silicon nitride particle diameter (3-10 μm), silicon nitride content (40-70 wt%), and binder material composition to achieve the target fracture toughness of 4.3 MPa·m^0.5 or more. This parameter optimization enables the heat-generating element to withstand repeated thermal stress without electrical disconnection while maintaining high heat resistance.

Inventive Principle:
Principle #35Parameter changes

2Speed

If the heat-generating portion is made thinner to enable rapid temperature rise, then heating speed is improved, but structural strength decreases

Engineering Contradiction:
Improvetemperature rise speedVSAvoidstructural strength
Core Design Contradiction:
SpeedVSStrength

Solution Approach 1:

The thin heat-generating portion maintains sufficient structural strength through the composite material structure, where silicon nitride ceramic particles provide thermal stability and the optimized binder material ensures mechanical integrity. This allows the portion to be made thinner for rapid heating while preventing brittleness and electrical disconnection.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

By optimizing the binder material composition and silicon nitride content ratio, the invention achieves high fracture toughness (4.3 MPa·m^0.5 or more) that enables the heat-generating portion to be made thinner without compromising structural strength, thus facilitating rapid temperature rise to 1,000°C or higher within one second.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The ceramic heater effectively prevents electrical disconnection during ultrahigh-speed temperature raising, ensuring a longer service life and enabling the rapid heating of the substrate surface to 1,000°C or higher within one second.

Implementation Method 1

a heater having an incorporated heat-generating element which generates heat through energization

Methodology Applied
Scientific EffectJoule heating: Joule Heating

Implementation Method 2

repeated application of a large thermal stress to the heat-generating element is responsible for the occurrence of an electrical disconnection in the heat-generating element

Methodology Applied
Scientific EffectThermal stress resistance: Thermal Shock

Data Source

PatentEP2608629B1Ceramic heater and manufacturing method therefor, and heating apparatus
Publication Date: 2017.07.19 NITERRA CO LTD
  • EP2608629B1 patent drawingFigure 1
  • EP2608629B1 patent drawingFigure 2A~2B
  • EP2608629B1 patent drawingFigure 3

AI summary

A ceramic heater having a substrate and a heat-generating element. The substrate is formed from an electrically insulating ceramic and extends rearward from the forward end of the ceramic heater in the direction of the axis. The heat-generating element has a heat-generating portion formed from an electrically conductive ceramic which contains silicon nitride and an electrically conductive material, disposed in a forward end portion of the substrate, and having a shape resembling the letter U as viewed along the direction of the axis. The heat-generating portion has a fracture toughness of 4.3 Mpa·m0.5 or more.