Silicon Oxide Mixture for Lithium Battery Negative Electrode

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Solution Overview

Problem

Silicon-based negative electrode active materials in lithium rechargeable batteries face volume expansion issues during charge and discharge, leading to reduced cycle-life due to crystalline structure changes, low conductivity, and small specific surface area, resulting in shorter battery life.

Innovation Solution

A negative electrode active material composed of a mixture of first and second silicon oxides with different particle diameters and specific surface areas, combined with a binder and a coating layer, to prevent volume change and maintain conductivity during charge and discharge cycles.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If silicon-based material is used as negative electrode active material, then high capacity is achieved, but volume expansion occurs during charge and discharge leading to reduced cycle-life

Engineering Contradiction:
Improvelithium storage capacityVSAvoidcycle-life
Core Design Contradiction:
Quantity of substanceVSDuration of action of stationary object

Solution Approach 1:

The negative electrode active material is divided into two distinct components: silicon particles (providing high capacity) and silicon oxide particles (providing structural stability). This segmentation allows each component to fulfill its specific function - silicon for capacity and silicon oxide for volume stability during charge-discharge cycles.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention creates a composite material system combining silicon and silicon oxide in specific weight ratios (70:30 to 90:10). This composite structure leverages the high capacity of silicon while the silicon oxide component compensates for volume expansion, achieving both high capacity and long cycle-life simultaneously.

Inventive Principle:
Principle #40Composite materials

2Duration of action of stationary object

If silicon oxide is used to reduce volume expansion, then cycle-life is improved, but electrical conductivity remains low

Engineering Contradiction:
Improvecycle-lifeVSAvoidelectrical conductivity
Core Design Contradiction:
Duration of action of stationary objectVSReliability

Solution Approach 1:

The invention optimizes the particle size parameters of both silicon and silicon oxide components. By controlling the D50 particle diameter within specific ranges (silicon: 3-10 μm, silicon oxide: 1-5 μm) and maintaining appropriate specific surface area ratios, the material achieves both low volume expansion and sufficient electrical conductivity for battery operation.

Inventive Principle:
Principle #35Parameter changes

3Volume of stationary object

If silicon oxide with small specific surface area is used, then volume expansion is reduced, but conductivity and reaction efficiency decrease

Engineering Contradiction:
Improvevolume stabilityVSAvoidelectrical conductivity
Core Design Contradiction:
Volume of stationary objectVSReliability

Solution Approach 1:

The invention precisely controls the specific surface area of silicon oxide particles (1-5 m²/g) and maintains an optimal specific surface area ratio between silicon and silicon oxide (5-50). This parameter optimization ensures that the silicon oxide provides sufficient volume stability while maintaining adequate conductivity and electrochemical reaction efficiency.

Inventive Principle:
Principle #35Parameter changes

Data Source

PatentEP2559660B1Negative electrode active material for rechargeable lithium battery, negative electrode including the same and method of preparing the same, and rechargeable lithium battery including the same
Publication Date: 2016.08.03 SAMSUNG SDI CO LTD
  • EP2559660B1 patent drawingFigure 1
  • EP2559660B1 patent drawingFigure 2~3
  • EP2559660B1 patent drawingFigure 4

AI summary

Provided are a negative electrode active material for a rechargeable lithium battery, which includes a first silicon oxide and a second silicon oxide with a particle diameter differing from the one of the first silicon oxide, a negative electrode including the negative electrode active material, and a method of manufacturing the negative electrode, and a rechargeable lithium battery including the negative electrode.