Silicon Oxide Intermediate Coating for Low-Loss Electrical Steel

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Solution Overview

Problem

Grain-oriented electrical steel sheets face challenges in achieving low iron loss and sufficient adhesion of insulation coatings, particularly due to interfacial unevenness caused by final-annealed films, which hinder magnetic properties and iron loss reduction.

Innovation Solution

A grain-oriented electrical steel sheet with a base steel sheet lacking a final-annealed film, featuring an intermediate layer of silicon oxide with a uniform thickness, ensuring strong adhesion of the insulation coating without the anchoring effects of uneven interfaces.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If a final-annealed film is formed on the base steel sheet to ensure coating adhesion, then the adhesion of insulation coating is improved, but the iron loss increases due to interfacial unevenness

Engineering Contradiction:
Improveadhesion of insulation coatingVSAvoidiron loss
Core Design Contradiction:
StrengthVSLoss of energy

Solution Approach 1:

The invention removes the final-annealed film from the steel sheet surface, extracting the source of interfacial unevenness that causes increased iron loss. Instead of forming a forsterite-based final-annealed film through conventional heat treatment, the patent uses a silicate-based coating applied at lower temperatures to provide adhesion without creating harmful interface irregularities.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention changes the chemical composition parameters of the coating from forsterite-based (Mg2SiO4) to silicate-based (containing SiO2 and other metal oxides), and changes the formation temperature from 600-1200°C to 200-600°C. This parameter change allows the coating to provide adhesion without creating the interfacial unevenness that increases iron loss.

Inventive Principle:
Principle #35Parameter changes

2Loss of energy

If the base steel sheet surface is smoothed to reduce iron loss, then the magnetic properties are improved, but the adhesion of insulation coating deteriorates

Engineering Contradiction:
Improveiron lossVSAvoidadhesion of insulation coating
Core Design Contradiction:
Loss of energyVSStrength

Solution Approach 1:

The silicate-based coating acts as an intermediary layer between the smoothed base steel sheet and the insulation coating. This intermediate coating provides the necessary adhesion function without requiring the interfacial unevenness that would otherwise be created by a final-annealed film, thus maintaining both low iron loss and good adhesion.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention uses a relatively thin silicate-based coating (1-10 μm) that serves the adhesion function effectively without creating persistent interface irregularities. This thinner, chemically different coating replaces the thicker final-annealed film and achieves adhesion through chemical bonding rather than mechanical anchoring.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Loss of energy

If a silicate-based coating is applied at low temperature to avoid final-annealed film formation, then the adhesion is improved and iron loss is reduced, but the coating process complexity increases

Engineering Contradiction:
Improveiron lossVSAvoidcoating process complexity
Core Design Contradiction:
Loss of energyVSDevice complexity

Solution Approach 1:

The invention combines the adhesion coating formation with the insulation coating application in a single process step. The silicate-based coating is applied and dried at low temperature (200-600°C) as part of the insulation coating process, merging what would otherwise be separate operations and reducing overall process complexity despite the specialized coating composition.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution results in improved adhesion of insulation coatings and reduced iron losses, enhancing magnetic properties and manufacturing efficiency by eliminating the need for final-annealed films and minimizing interfacial stress concentrations.

Implementation Method 1

an intermediate layer that is disposed on a surface of the base steel sheet and mainly contains silicon oxide

Methodology Applied
Scientific EffectAdhesion: Adhesive

Implementation Method 2

a coating is formed on a surface of a base steel sheet to apply tension to the base steel sheet to reduce the iron loss

Methodology Applied
Scientific EffectTension: Tension

Implementation Method 3

baking and drying the coating solution within a temperature range of 300°C to 950°C for 10 seconds or longer

Methodology Applied
Scientific EffectBaking: Heat Treatment

Data Source

PatentEP3913075B1Grain-oriented electrical steel sheet and method for manufacturing same
Publication Date: 2024.08.07 NIPPON STEEL CORPORATION
  • EP3913075B1 patent drawingFigure 1~2

AI summary

This grain-oriented electrical steel sheet has a base steel sheet in which a final-annealed film is substantially not present on a surface, an intermediate layer that is disposed on a surface of the base steel sheet and mainly contains silicon oxide, and an insulation coating disposed on a surface of the intermediate layer. In the intermediate layer, a value obtained by dividing a standard deviation σ of a thickness of the intermediate layer by an average value T of the thickness of the intermediate layer is 0.500 or less.