Silicon Precursor for High-Temperature ALD Step Coverage

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Solution Overview

Problem

Conventional silicon precursors fail to produce high-quality silicon-containing thin films at high process temperatures, particularly due to issues with step coverage, thickness control, and impurity contamination, limiting their application in advanced semiconductor devices.

Innovation Solution

A novel silicon precursor compound, represented by specific chemical formulas, is introduced for use in vapor deposition methods like ALD and CVD, which is thermally stable at 600 °C or more, ensuring low impurity concentration and excellent step coverage, and can be used to manufacture thin films with precise thickness control and uniform deposition rates.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional silicon precursors are used for deposition, then the deposition process can be performed, but the step coverage and thickness control are poor and impurities are contained in the thin film

Engineering Contradiction:
Improvethickness controlVSAvoidimpurity concentration
Core Design Contradiction:
Manufacturing precisionVSReliability

Solution Approach 1:

The patent modifies the chemical structure of silicon precursor molecules by changing parameters such as the type and position of substituent groups (e.g., using specific aminosilane structures with controlled steric hindrance and reactivity). This allows optimization of deposition characteristics to achieve better thickness control and reduced impurity incorporation in the resulting thin films

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention employs composite molecular structures combining silicon centers with specifically designed organic ligands and substituent groups. These composite precursor molecules exhibit synergistic properties that enable simultaneous improvement of step coverage, thickness uniformity, and film purity during deposition processes

Inventive Principle:
Principle #40Composite materials

2Manufacturing precision

If conventional silicon precursors are used, then deposition can proceed, but excellent step coverage and surface characteristics cannot be ensured

Engineering Contradiction:
Improvestep coverageVSAvoidprocess complexity
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The patent optimizes molecular parameters of silicon precursors including steric hindrance, reactivity, and volatility to achieve excellent step coverage. By carefully selecting substituent groups and their positions on the silicon molecule, the precursors deposit uniformly on complex three-dimensional structures with high aspect ratios, providing conformal coverage without requiring complex process modifications

Inventive Principle:
Principle #35Parameter changes

3Productivity

If high process temperature is used for deposition, then deposition rate increases, but impurity concentration increases and film quality deteriorates

Engineering Contradiction:
Improvedeposition rateVSAvoidfilm quality
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent designs silicon precursor molecules with specific thermal stability characteristics by selecting appropriate substituent groups and molecular architectures. These modified precursors maintain structural integrity at elevated deposition temperatures, enabling high deposition rates while preventing thermal decomposition that would otherwise introduce impurities and degrade film quality

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The novel silicon precursor enables the production of high-quality silicon-containing thin films with low impurity levels and excellent surface characteristics, suitable for applications in 3D-NAND memory devices, semiconductors, displays, and solar cells, with expected improvements in interface characteristics and corrosion resistance.

Implementation Method 1

a vapor deposition precursor which comprises any one or more compounds selected from the group consisting of a compound represented by Formula 1

Methodology Applied
Scientific EffectVapor deposition: Physical Vapour Deposition

Implementation Method 2

chemical vapor deposition (CVD)

Methodology Applied
Scientific EffectChemical vapor deposition: Chemical Vapour Deposition

Implementation Method 3

atomic layer deposition (ALD)

Methodology Applied
Scientific EffectAtomic layer deposition: Chemical Vapour Deposition

Data Source

PatentEP3766888A1Silicon precursor and method of manufacturing silicon-containing thin film using the same
Publication Date: 2021.01.20 HANSOL CHEM
  • EP3766888A1 patent drawingFigure 1
  • EP3766888A1 patent drawingFigure 2
  • EP3766888A1 patent drawingFigure 3

AI summary

The present invention relates to a vapor deposition compound capable of thin film deposition through vapor deposition, and particularly to a silicon precursor capable of being applied to ALD or CVD, and specifically, enabling high temperature deposition, and a method of manufacturing a silicon-containing thin film.