Silicon-Tin Alloy Electrodes for Lithium-Ion Batteries

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Solution Overview

Problem

Metal alloy anodes for lithium-ion batteries exhibit poor cycle life and coulombic efficiency due to fragmentation during compositional changes, which is not effectively addressed by existing technologies.

Innovation Solution

An electrode composition with a multi-phase microstructure of silicon, metal silicide, and silicon carbide, combined with a binder and conductive diluent, is developed, featuring an amorphous and nanocrystalline phase structure, specifically formulated as Si x Sn q M y C z, where q, x, y, and z represent atomic percent values, and M includes metals like manganese, molybdenum, and cobalt, prepared through high-shear ball-milling.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If metal alloys are used as anodes for lithium ion batteries, then capacity is improved, but cycle life and coulombic efficiency deteriorate due to fragmentation during expansion and contraction

Engineering Contradiction:
ImprovecapacityVSAvoidcycle life and coulombic efficiency
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The alloy is segmented into a composite structure consisting of metal alloy particles dispersed within a porous carbon matrix. This segmentation allows the carbon matrix to independently bear the mechanical stress of expansion and contraction, protecting the alloy particles from fragmentation while maintaining high capacity.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

A composite material structure is formed by combining metal alloy particles with a porous carbon matrix. The carbon component provides structural stability and conductivity, while the alloy particles provide high capacity, achieving both high capacity and good cycle life simultaneously.

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If alloy particles undergo compositional changes during lithium insertion and extraction, then capacity is improved, but structural integrity deteriorates leading to fragmentation

Engineering Contradiction:
ImprovecapacityVSAvoidstructural integrity
Core Design Contradiction:
Quantity of substanceVSStrength

Solution Approach 1:

The porous carbon matrix serves as a pre-established protective cushion surrounding the alloy particles. This carbon matrix is designed beforehand to accommodate the volume changes during lithium insertion and extraction, preventing direct mechanical stress on the alloy particles and thus preventing fragmentation.

Inventive Principle:
Principle #11Beforehand cushioning (Prior cushioning)

Solution Approach 2:

A porous carbon matrix is used to host the alloy particles. The porous structure provides sufficient space for the alloy particles to expand and contract during lithium insertion and extraction without experiencing excessive mechanical stress, thereby maintaining structural integrity while enabling high capacity.

Inventive Principle:
Principle #31Porous materials

Data Source

PatentEP1974408B1Silicon-containing alloys useful as electrodes for lithium-ion batteries
Publication Date: 2017.06.21 3M INNOVATIVE PROPERTIES CO

AI summary

An electrode composition for a lithium ion battery having the formula SixSnqMyCz where q, x, y, and z represent atomic percent values and (a) (q + x) > 2y + z; (b) q ≥ 0, (c) z ≥0; and (d) M is one or more metals selected from manganese, molybdenum, niobium, tungsten, tantalum, iron, copper, titanium, vanadium, chromium, nickel, cobalt, zirconium, yttrium, or a combination thereof. The Si, Sn, M, and C elements are arranged in the form of a multi-phase microstructure comprising: (a) an amorphous phase comprising silicon; (b) a nanocrystalline phase comprising a metal suicide; and (c) a phase comprising silicon carbide phase when z > 0; and (d) an amorphous phase comprising Sn when q > 0.