Multilayer Silicone Composite Thickness Control

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Solution Overview

Problem

Existing methods for producing multilayer silicone composites fail to achieve precise and uniform layer thicknesses, leading to inadequate mechanical properties and increased production costs, particularly in continuous processes for applications like dielectric electroactive polymers.

Innovation Solution

A continuous method using a multistep process with an angled slot die and controlled travel speed, applying solvent-containing or solvent-free silicone compositions, followed by solvent removal and partial or full crosslinking, to achieve layer thicknesses between 0.1 and 200 μm with ±5% precision over 200 cm², enhancing mechanical properties and surface quality.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional coating techniques (roller coating, air doctor, reverse roll coating, wire-wound bar coating, spray coating) are used to produce thin silicone films, then film production is achieved, but thickness precision is insufficient

Engineering Contradiction:
Improvethickness precisionVSAvoidproduction complexity
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The patent changes the physical parameters of the coating process by using a doctor blade with a specific geometry and material properties that enable precise thickness control. The doctor blade parameters (angle, width, material) are optimized to achieve uniform thin film deposition with precision better than conventional coating methods, directly resolving the thickness precision issue while maintaining ease of manufacture through a straightforward coating process

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces complex mechanical coating systems with a simpler doctor blade mechanism that provides superior thickness control. The doctor blade system substitutes for multiple complex coating apparatuses while achieving better manufacturing precision through its straightforward mechanical action of scraping excess material to leave a uniform thin film

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Manufacturing precision

If casting processes are used to produce thin silicone films, then film production is achieved, but thickness precision and production efficiency are insufficient

Engineering Contradiction:
Improvethickness precisionVSAvoidproduction efficiency
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The patent implements a continuous coating process where the doctor blade operates continuously on moving substrate material, enabling high production efficiency. The process maintains continuous useful action by continuously depositing uniform thin silicone films without interruption, unlike batch casting processes, thereby simultaneously achieving both thickness precision and high productivity

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The patent changes the process parameters from batch casting to continuous coating by controlling the speed of substrate movement and the rate of material application. This parameter optimization enables the doctor blade to maintain consistent film thickness while operating continuously, resolving both the precision and efficiency shortcomings of casting processes

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If extrusion methods are used for HTV rubbers, then production is achieved, but layer thickness variations and limited thickness reduction capability exist

Engineering Contradiction:
Improvelayer thickness uniformityVSAvoidplant design complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent replaces complex extrusion plant systems with a simpler doctor blade coating system that achieves superior layer thickness uniformity. The doctor blade mechanism substitutes for multi-component extrusion equipment, providing better control over thin film thickness while reducing device complexity through its straightforward scraping action that naturally produces uniform layers

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent changes the critical parameters of the coating process by optimizing the doctor blade geometry (angle, width, edge profile) and operational parameters (speed, pressure, material viscosity) to achieve uniform thin film deposition. These parameter optimizations enable precise control of layer thickness down to very thin dimensions, resolving the thickness uniformity and reduction capability issues of extrusion methods while simplifying plant design

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method enables the production of multilayer silicone composites with high precision, improved mechanical stability, and long-term load resistance, suitable for applications in actuators, sensors, and generators, while reducing production costs and variations in layer thickness.

Implementation Method 1

a solvent-containing or solvent-free, crosslinkable silicone composition (X) is applied through the slot of a slot die to a moving carrier

Methodology Applied
Scientific EffectCapillary action: Capillary Action

Implementation Method 2

a solvent-containing or solvent-free, crosslinkable silicone composition (X) is applied through the slot of a slot die to a moving carrier

Methodology Applied
Scientific EffectSurface tension: Surface Tension

Implementation Method 3

subsequently the solvent, if present, is removed from the silicone layer which forms on the carrier film

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 4

the silicone layer is partially or wholly crosslinked

Methodology Applied
Scientific EffectCrosslinking: Chemical Bonding

Data Source

PatentUS10518455B2Method for producing silicone multi-layer composites
Publication Date: 2019.12.31 WACKER CHEMIE AG
  • US10518455B2 patent drawing
  • US10518455B2 patent drawing
  • US10518455B2 patent drawing

AI summary

Multilayer silicone composites with precise thickness are produced by sequential extrusion of curable silicone films, and partially but not fully crosslinking a preceding silicone film prior to extruding a next subsequent film.