Silicone Rubber Flame Coating Adhesion Reduction

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Solution Overview

Problem

Existing methods for reducing the stickiness of silicone rubber surfaces, particularly in medical applications like catheter tubes, are either cost-intensive or unsuitable for molded parts and clean room conditions, and often require additional treatments or complex equipment.

Innovation Solution

A pyrolytic method depositing a 40-100 nm thick silicate-containing layer from an organosilicon compound, using a flame coating process at atmospheric pressure, which effectively reduces adhesion and stickiness on silicone rubber surfaces without the need for subsequent treatments.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-generated harmful factors

If release agents or talc are applied to reduce stickiness, then adhesion is reduced, but manufacturing cost increases and clean room consolidation becomes difficult

Engineering Contradiction:
ImproveadhesionVSAvoidmanufacturing cost
Core Design Contradiction:
Object-generated harmful factorsVSEase of manufacture

Solution Approach 1:

The silicate layer is applied during the molding process itself, before the article leaves the production line. This preliminary treatment eliminates the need for subsequent release agent application, reducing manufacturing steps and costs while maintaining low adhesion properties throughout the product lifecycle

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The silicate-containing master batch is mixed into the silicone rubber compound during compounding, allowing the material to self-modify its surface properties during processing. The silicate layer forms automatically on the surface during molding, eliminating the need for separate coating or treatment steps

Inventive Principle:
Principle #25Self-service

2Object-generated harmful factors

If plasma polymerisation is used to deposit coating, then adhesion is reduced, but the process becomes vacuum-based and extremely cost-intensive

Engineering Contradiction:
ImproveadhesionVSAvoidprocess complexity
Core Design Contradiction:
Object-generated harmful factorsVSDevice complexity

Solution Approach 1:

The patent replaces the complex plasma polymerisation system with a simple flame coating process. Instead of using vacuum plasma generation equipment, the invention uses a flame source to deposit silicate layer, dramatically simplifying the device requirements while achieving the same adhesion reduction effect

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent changes the operating conditions from vacuum plasma environment to atmospheric pressure flame environment. This parameter change allows the coating process to occur under normal atmospheric conditions, eliminating the need for vacuum equipment and reducing process complexity

Inventive Principle:
Principle #35Parameter changes

3Strength

If pyrolysis process with SiOx-C adhesion promoter is used, then adhesion is improved, but additional temperature control system and silane application system are required

Engineering Contradiction:
ImproveadhesionVSAvoidequipment complexity
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The patent combines the adhesion promotion function with the surface coating function into a single integrated flame coating process. The silicate-containing master batch is incorporated during compounding, and the flame coating simultaneously applies the silicate layer and creates the adhesion-promoting surface chemistry, eliminating the need for separate SiOx-C application systems

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The silicate-containing master batch acts as an intermediary that carries the adhesion-promoting silicate particles throughout the silicone rubber compound. This intermediary approach allows the adhesion promotion function to be distributed within the material itself rather than requiring separate application equipment

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method provides a cost-effective, adhesion-free silicone rubber surface suitable for both profiles and molded parts, significantly reducing friction and adhesion, and can be integrated into production lines, ensuring efficient and clean processing, especially in medical applications.

Implementation Method 1

A pyrolytic method depositing a 40-100 nm thick silicate-containing layer from an organosilicon compound

Methodology Applied
Scientific EffectPyrolysis: Pyrolysis

Implementation Method 2

Flame coating is carried out using a burner. As the film-forming gas, an alkoxysilane compound or tetramethylsilane is mentioned

Methodology Applied
Scientific EffectFlame coating: Heating

Data Source

PatentEP1882052B1Method for modifying a silicone rubber surface
Publication Date: 2012.08.01 RAUMEDIC AG
  • EP1882052B1 patent drawingFigure 1
  • EP1882052B1 patent drawingFigure 2
  • EP1882052B1 patent drawingFigure 3a

AI summary

Disclosed is a method for modifying a silicone rubber surface by coating the same with a functional layer. Said method is characterized in that a silicate-containing functional layer is deposited on the silicon rubber surface from a flame, whereby the surface is modified so as to be provided with very low adhesion or tackiness.