Liquid Silicone Rubber Extrusion with Coriolis Mass Flow Control

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Solution Overview

Problem

Current methods for producing liquid silicone rubber compositions face challenges in maintaining consistent mass flow and quality due to variations in material density and the presence of air bubbles, leading to inefficiencies and increased complexity in batch processes.

Innovation Solution

A manufacturing assembly that includes a preconditioning unit, a primary mass flow meter, an extruder with multiple introduction ports, and a control system to monitor and adjust the mass flow of silicone rubber base material and additives, ensuring accurate proportions and consistent output.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If batch processes are used to provide smaller batch quantities of liquid silicone rubber, then flexibility in composition and waste of time/materials is minimized, but productivity and process efficiency are reduced

Engineering Contradiction:
Improveflexibility in compositionVSAvoidprocess efficiency
Core Design Contradiction:
Adaptability or versatilityVSProductivity

Solution Approach 1:

The continuous extrusion process is segmented into multiple functional zones along the extruder length, including a preconditioning zone for base material, a deaeration zone for removing air bubbles, and a compounding zone for adding additives. This segmentation allows the system to maintain continuous high productivity while accommodating different composition requirements through controlled material introduction at different stages.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The system employs dynamic control of material flow rates and additive introduction timing to adapt to different composition requirements. The extrusion process continuously adjusts parameters such as screw speed, barrel temperature, and additive feed rates to optimize both productivity and composition flexibility for different product specifications.

Inventive Principle:
Principle #15Dynamics

2Productivity

If continuous processes are used to increase productivity, then process efficiency is improved, but quality consistency deteriorates due to problems in metering and feeding

Engineering Contradiction:
Improveprocess efficiencyVSAvoidquality consistency
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The system incorporates feedback control through Coriolis mass flow meters that continuously monitor the actual mass flow of liquid silicone rubber entering the extruder. The control system uses this real-time data to adjust pump delivery rates and compensate for density variations, ensuring consistent additive proportions and maintaining quality consistency throughout continuous production.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The invention replaces traditional volumetric metering pumps with Coriolis mass flow measurement and control systems. This substitution transitions from mechanical volume-based metering to precise mass-based measurement and control, eliminating the quality consistency problems associated with volumetric measurement of materials with variable density.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Device complexity

If metering pumps with known pumping volumes are used to determine master flow, then device complexity is reduced, but measurement precision deteriorates due to variability in material density and air bubbles

Engineering Contradiction:
Improvesystem simplicityVSAvoidmass flow accuracy
Core Design Contradiction:
Device complexityVSMeasurement precision

Solution Approach 1:

The system replaces simple volumetric metering pumps with Coriolis mass flow meters that directly measure mass flow rate. This substitution eliminates the measurement errors caused by density variations and air bubble presence, providing accurate mass flow data for control purposes while maintaining relatively simple system architecture.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The invention changes the measurement parameter from volume (which is affected by density and air bubbles) to mass flow rate using Coriolis effect-based measurement. This parameter change enables accurate flow measurement and control despite variations in material density and the presence of air bubbles in the liquid silicone rubber.

Inventive Principle:
Principle #35Parameter changes

4Adaptability or versatility

If cleaning and switching are performed to accommodate compositions of different type, then adaptability is improved, but device complexity and initial investment increase due to more accessories

Engineering Contradiction:
Improvecomposition type flexibilityVSAvoidprocess complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The system maintains continuous extrusion operation when changing composition types by using a build-up/clearance strategy. Different composition batches are continuously processed through the extruder, with the control system managing transition periods where material is gradually introduced and cleared. This approach eliminates the need for complete system shutdowns and extensive cleaning operations, reducing complexity while maintaining adaptability.

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This solution enables continuous production of liquid silicone rubber compositions with high accuracy and flexibility, reducing waste and the need for extensive cleaning and mixing steps, while maintaining quality consistency across varying conditions.

Implementation Method 1

a primary Coriolis mass flow meter downstream of the preconditioning assembly and upstream of the extruder

Methodology Applied
Scientific EffectCoriolis effect: Coriolis Force

Implementation Method 2

an extruder device, having a first introduction port adapted for the introduction of silicone rubber base material

Methodology Applied
Scientific EffectShear mixing: Shear Stress

Data Source

PatentUS11820895B2Process and apparatus to make liquid silicone rubber compositions
Publication Date: 2023.11.21 DOW SILICONES CORP
  • US11820895B2 patent drawing

AI summary

Provided are an assembly and process for the continuous or semi-continuous preparation of addition-crosslinking liquid silicone rubbers and to liquid silicone rubber compositions made therefrom. Also disclosed are articles made from the liquid silicone rubber compositions.