Silver-Beta Zeolite Filtration for Alcoholic Beverage Purification

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Solution Overview

Problem

Current methods for removing unwanted components like sulfur compounds and pyridine from alcoholic beverages during storage are inefficient, leading to product loss and quality issues, as they do not effectively address the removal of specific compounds such as dimethyl sulfide, dimethyl disulfide, and dimethyl trisulfide.

Innovation Solution

A metal-supported zeolite, specifically with silver as the metal component supported on beta-type or Y-type zeolites, is used to filter alcoholic beverages, effectively removing unwanted components like dimethyl sulfide, dimethyl disulfide, and pyridine while maintaining flavor components, with a liquid-hourly space velocity of 1-30 h^-1 and a temperature range of -20 to 100 °C.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If traditional storage methods are used to mature alcoholic beverages, then the beverages develop intrinsic taste through spontaneous chemical reactions, but product loss increases due to evaporation and absorption by barrels

Engineering Contradiction:
Improvequality of alcoholic beverageVSAvoidamount of raw whisky
Core Design Contradiction:
ReliabilityVSLoss of substance

Solution Approach 1:

The patent applies preliminary action by proactively removing unwanted components (sulfur compounds, pyridine, etc.) from the alcoholic beverage before storage, rather than waiting for spontaneous changes during long-term storage. This pre-treatment approach eliminates harmful substances early in the process, reducing the need for extended storage periods and thereby minimizing evaporation losses and barrel absorption.

Inventive Principle:
Principle #10Preliminary action

2Reliability

If storage period is prolonged to remove unwanted components naturally, then quality improves through maturation, but productivity decreases due to increased product loss

Engineering Contradiction:
Improvequality of alcoholic beverageVSAvoidproduction efficiency
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The patent implements preliminary action by using a metal-supported zeolite catalyst to pre-remove unwanted components (sulfur compounds, pyridine, etc.) before storage. This eliminates the need for prolonged storage periods required for natural maturation, thereby significantly reducing evaporation losses and improving production efficiency while still achieving high-quality products.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent applies parameter changes by introducing a catalyst (metal-supported zeolite) that alters the chemical environment of the alcoholic beverage. This catalytic approach enables rapid removal of unwanted components through enhanced adsorption and chemical reactions, replacing the slow natural maturation process and reducing storage time requirements.

Inventive Principle:
Principle #35Parameter changes

3Loss of substance

If existing adsorbent methods are used to remove unwanted components, then some purification is achieved, but removal efficiency of specific compounds (dimethyl sulfide, pyridine) is insufficient

Engineering Contradiction:
Improveunwanted componentsVSAvoidremoval efficiency
Core Design Contradiction:
Loss of substanceVSReliability

Solution Approach 1:

The patent applies composite materials by using a metal-supported zeolite catalyst, which combines metal particles (with catalytic activity) and zeolite (with adsorption properties). This composite structure provides both adsorption capacity for sulfur compounds and catalytic activity for converting pyridine and other nitrogen-containing compounds, achieving superior removal efficiency compared to single-material adsorbents.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent applies parameter changes by introducing a catalyst that modifies the chemical reactivity of the system. The metal-supported zeolite changes the chemical environment to enhance the removal of specific compounds through catalytic reactions, going beyond simple physical adsorption to achieve more effective purification of refractory compounds like pyridine.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method efficiently removes unwanted sulfur compounds and pyridine from various types of alcoholic beverages, reducing product loss and enhancing quality by maintaining the flavor profiles of the beverages.

Implementation Method 1

a method of bringing alcoholic beverages into contact with an adsorbent prepared by processing silica with an organic silane compound

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

a metal-supported zeolite in which a metal component is supported on a zeolite, wherein the metal component is silver and the zeolite is selected from a beta-type and a Y-type

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentEP3088508B1Alcoholic beverage manufacturing method
Publication Date: 2020.10.21 IDEMITSU KOSAN CO LTD
  • EP3088508B1 patent drawing
  • EP3088508B1 patent drawing

AI summary

The metal-supported zeolite for alcoholic beverages of the present invention is a zeolite that carries a metal component, wherein the metal component is silver, and the zeolite is at least one selected from a beta-type one and a Y-type one. The metal-supported zeolite is for removing unwanted components contained in alcoholic beverages.