Silver-Carbon Adhesive X-Ray Window for Hermetic Conductive Sealing

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Solution Overview

Problem

Existing x-ray windows face challenges in achieving a balance of low gas permeability, high strength, low visible and infrared light transmission, high x-ray flux, corrosion resistance, reliability, cost-effectiveness, thermal durability, and compatibility, while maintaining a hermetic seal and electrical conductivity, especially when subjected to differential pressures and temperature fluctuations.

Innovation Solution

The x-ray window design incorporates a thin film mounted by an adhesive to a housing, where the adhesive is composed of a combination of materials such as silver, carbon, graphene, epoxy resin, methyl-5-norbornene-2,3-dicarboxylic anhydride, glycerol, trimellitic anhydride, and imidazole, which provides a hermetic seal, high electrical conductivity, and mechanical strength, while optimizing weight percentages for balanced properties like thermal conductivity and cost-effectiveness.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a hermetic seal is implemented using traditional adhesives, then gas permeability is reduced, but electrical conductivity and mechanical strength deteriorate

Engineering Contradiction:
Improvehermetic sealVSAvoidmechanical strength
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The patent uses a composite adhesive material containing silver particles (for electrical conductivity), carbon particles (for mechanical strength and conductivity), and epoxy resin matrix (for hermetic sealing and structural integrity). This composite formulation simultaneously achieves hermetic seal, electrical conductivity, and mechanical strength by combining materials with complementary properties.

Inventive Principle:
Principle #40Composite materials

2Reliability

If low atomic number materials are used for high x-ray transmission, then x-ray flux is improved, but structural strength and durability worsen

Engineering Contradiction:
Improvex-ray transmissionVSAvoidstructural strength
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The patent employs an amorphous carbon thin film that is sufficiently thin to transmit low-energy x-rays effectively while being strong enough to withstand differential pressures. The thin film structure allows x-ray photons to pass through with minimal attenuation while maintaining structural integrity through optimized thickness and material properties.

Inventive Principle:
Principle #30Flexible shells and thin films

Solution Approach 2:

The x-ray window uses a composite structure combining amorphous carbon thin film with adhesive materials containing silver and carbon particles. This composite approach allows the thin film to provide x-ray transmission while the adhesive composite provides structural support and mechanical strength.

Inventive Principle:
Principle #40Composite materials

3Reliability

If thin films are used to reduce weight and improve transmission, then x-ray flux and weight are improved, but mechanical strength and vacuum withstanding capability worsen

Engineering Contradiction:
Improvex-ray transmissionVSAvoidpressure withstanding capability
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The patent creates a composite adhesive system containing silver particles, carbon particles, and epoxy resin that bonds the thin film to the housing. This composite adhesive provides both mechanical strength to support the thin film under differential pressure and electrical conductivity for charge dissipation, while allowing the thin film to remain thin for optimal x-ray transmission.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent optimizes the thickness of the amorphous carbon film to balance x-ray transmission and mechanical strength. By controlling the film thickness parameter, the design achieves sufficient transparency to low-energy x-rays while maintaining adequate strength to withstand vacuum differential pressures when bonded with the adhesive composite.

Inventive Principle:
Principle #35Parameter changes

4Reliability

If high electrical conductivity materials are used, then electrical conductivity is improved, but visible and infrared light transmission increases

Engineering Contradiction:
Improveelectrical conductivityVSAvoidlight transmission
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent uses silver and carbon particles distributed locally within the adhesive material at the bonding interface, rather than using a continuous metallic layer. This localized incorporation provides sufficient electrical conductivity for charge dissipation while the adhesive matrix and particle distribution minimize visible and infrared light transmission by scattering and absorbing photons.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration results in an x-ray window that effectively transmits low-energy x-rays, withstands high temperatures, and maintains a reliable vacuum, ensuring high reliability and durability while reducing costs, with improved mechanical and electrical properties.

Implementation Method 1

X-ray windows are designed to transmit a high percent of x-rays, even low energy x-rays

Methodology Applied
Scientific EffectX-ray transmission: X-Ray

Implementation Method 2

high electrical conductivity. Each x-ray window design is a balance between these characteristics

Methodology Applied
Scientific EffectElectrical conduction: Conduction (electrical)

Data Source

PatentUS20240417597A1Silver - carbon adhesive for x-ray window
Publication Date: 2024.12.19 MOXTEK INC
  • US20240417597A1 patent drawing
  • US20240417597A1 patent drawing

AI summary

An x-ray window comprises a housing with a flange encircling an aperture. A thin film is located on the flange and spans the aperture. An adhesive is between an outer ring of the thin film and the flange. The adhesive mounts the thin film to the housing. The adhesive comprises silver and carbon.