Simulated Moving Bed Bypass Lines for Separation Yield

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Solution Overview

Problem

Simulated moving bed (SMB) separation devices face challenges in minimizing pollution and compositional discontinuities due to fluid mixing and re-circulation during operational sequence changes, particularly when fluid streams with different compositions are used for flushing, which disrupts the ideal concentration profile and efficiency of separation processes.

Innovation Solution

The SMB device employs a configuration where bypass lines connected to injection or withdrawal lines in operation establish flushing flows regulated at 50% of the synchronicity flow rate, with specific flow corrections in different portions of the bypass lines to maintain fluid composition continuity, reducing re-circulation and dead zones, and enhancing the yield of desired products.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If bypass lines are used for flushing during operational sequence changes, then fluid mixing and re-circulation are reduced, but compositional discontinuities and pollution occur due to different fluid compositions

Engineering Contradiction:
Improveseparation efficiencyVSAvoidcompositional discontinuities
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The invention changes the flow rate parameter of the flushing fluid in bypass lines to 50% of the synchronicity flow rate. This parameter adjustment optimizes the balance between reducing fluid mixing/re-circulation and maintaining compositional continuity, thereby resolving the contradiction between separation efficiency and compositional discontinuities

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention applies partial flushing action by using bypass lines that carry a controlled portion (50% of synchronicity flow rate) of the flushing fluid, rather than complete flushing. This partial action reduces harmful fluid mixing while maintaining sufficient compositional continuity

Inventive Principle:
Principle #16Partial or excessive action

2Productivity

If flushing flow rates are increased to reduce dead zones and re-circulation, then operational performance improves, but compositional discontinuities increase due to higher fluid mixing

Engineering Contradiction:
Improveoperational performanceVSAvoidfluid composition continuity
Core Design Contradiction:
ProductivityVSStability of the object's composition

Solution Approach 1:

The invention optimizes the flushing flow rate parameter to exactly 50% of the synchronicity flow rate. This specific parameter value achieves the optimal balance between reducing dead zones and maintaining compositional stability, resolving the contradiction between productivity and composition continuity

Inventive Principle:
Principle #35Parameter changes

3Reliability

If bypass lines connect all successive plates, then flushing coverage is maximized, but device complexity and flow control difficulty increase

Engineering Contradiction:
Improveflushing effectivenessVSAvoidbypass line configuration
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The invention segments the bypass line network by connecting only alternate successive plates (e.g., plates 1-3, 3-5, 5-7) rather than all successive plates. This segmentation reduces device complexity and flow control difficulty while maintaining sufficient flushing effectiveness through the distributed bypass connections

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach results in a significant gain in the yield of the desired product, improving the operational performance and purity of separations, such as para-xylene and meta-xylene, by minimizing compositional discontinuities and maintaining fluid composition continuity throughout the separation process.

Implementation Method 1

a column (and frequently two) divided into several successive beds of adsorbant Ai

Methodology Applied
Scientific EffectAdsorption: Adsorption

Data Source

PatentUS8123951B2Process and apparatus for simulated moving bed separation comprising bypass lines in every other bed and with controlled flushing flow rates during injections and withdrawals
Publication Date: 2012.02.28 IFP ENERGIES NOUVELLES
  • US8123951B2 patent drawing
  • US8123951B2 patent drawing
  • US8123951B2 patent drawing

AI summary

A process for separating a feed F by simulated moving bed adsorption in a SMB device comprises external bypass lines Li/i+1 which directly connect two successive plates, Pi, Pi+1, the index ā€œiā€ being either even or (exclusive of the foregoing) odd, along the whole length of the column, allowing said plates to be flushed, in which each of the bypass lines Li/i+1 comprises automated means for regulating the flow rate in the bypass lines, the bypass lines in certain cases being subject to a flushing flow during injection or withdrawal operations.