Automated Simultaneous Process Control for Continuous Protein Purification

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

In continuous protein purification processes, maintaining specific pH and conductivity levels while managing the fill level of intermediate surge tanks is challenging due to interdependent process characteristics and occasional interruptions in the input stream, requiring an advanced automated control strategy to maintain tight operation limits.

Innovation Solution

Implementing a method for automated simultaneous control of multiple process characteristics using a combination of feed forward regulation and feedback control, with subsystems for controlling multiple actuators influencing the same conditioning volume, allowing for real-time adjustments of pH, conductivity, and fill level management.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If multiple actuators are controlled simultaneously to adjust pH and conductivity in a surge tank, then process characteristics can be maintained within acceptable ranges, but the complexity of the control system increases

Engineering Contradiction:
Improveprocess characteristic control precisionVSAvoidcontrol system complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The control system is segmented into multiple independent control loops, each responsible for a specific process characteristic (pH, conductivity, fill level). Each loop independently controls its designated actuator based on sensor feedback, avoiding the complexity of coordinating multiple actuators simultaneously while maintaining precise control of each parameter

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The system performs preliminary detection and calculation for each actuator before actuation. Sensors continuously monitor process characteristics, the control system calculates required adjustments in advance, and actuators are commanded sequentially based on pre-computed values, simplifying the control logic while maintaining precision

Inventive Principle:
Principle #10Preliminary action

2Manufacturing precision

If tight operation limits are maintained for all process characteristics, then product quality is ensured, but the system becomes less adaptable to input stream interruptions

Engineering Contradiction:
Improveoperation limit controlVSAvoidadaptability to interruptions
Core Design Contradiction:
Manufacturing precisionVSAdaptability or versatility

Solution Approach 1:

The system employs continuous feedback control where sensors monitor process characteristics and feed this information back to the control system. When interruptions occur, the feedback mechanism detects deviations from setpoints and automatically adjusts actuators to restore tight operation limits, thereby maintaining both precision and adaptability

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The control system dynamically adapts its behavior based on real-time conditions. During normal operation, it maintains tight control limits; when interruptions are detected, it dynamically adjusts control parameters and actuator responses to handle the abnormal situation while striving to return to tight control once normal conditions resume

Inventive Principle:
Principle #15Dynamics

3Manufacturing precision

If pH and conductivity set agents are added to adjust process characteristics, then the next unit operation requirements are met, but the fill level of the surge tank becomes difficult to control

Engineering Contradiction:
Improveprocess characteristic adjustmentVSAvoidsurge tank fill level
Core Design Contradiction:
Manufacturing precisionVSQuantity of substance

Solution Approach 1:

The control of fill level is segmented into a separate control loop independent of pH and conductivity control. A dedicated sensor monitors fill level and a separate actuator (such as a discharge pump or valve) is controlled based on fill level measurements, while pH and conductivity control use their own actuators. This segmentation prevents the fill level from becoming difficult to control when chemical agents are added

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The surge tank fill level acts as an intermediary variable that mediates between the addition of set agents and the output stream requirements. By independently controlling the fill level through a separate feedback loop, the system uses the fill level as a buffer to accommodate the volume changes caused by adding pH and conductivity set agents without compromising the quality of the output stream

Inventive Principle:
Principle #24Intermediary (Mediator)

Data Source

PatentEP3931642B1Automated simultaneous process control
Publication Date: 2024.07.03 BAYER AG
  • EP3931642B1 patent drawingFigure 1
  • EP3931642B1 patent drawingFigure 2
  • EP3931642B1 patent drawingFigure 3

AI summary

Described herein is a method and a system for automated simultaneous control of at least two process characteristics of a continuous production process with at least one fluid stream, at least two unit operations, at least one process control system and at least one conditioning volume.