Single-Crystalline Work Piece Production via Epitaxial Growth

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Solution Overview

Problem

Current methods for producing three-dimensional work pieces with single-crystalline microstructures using powder bed fusion struggle to consistently achieve high-quality single-crystalline materials, particularly in complex geometries, due to limitations in controlling microstructure formation during the additive layering process.

Innovation Solution

A method involving the use of a substantially single-crystalline substrate and controlled irradiation of raw material powder layers with electromagnetic or particle radiation, adjusting parameters such as beam size, exposure time, and crystal orientation to promote single-crystalline growth and metallurgical bonding, ensuring a consistent single-crystalline microstructure across the work piece.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If conventional powder bed fusion methods are used to produce three-dimensional work pieces, then manufacturing complexity is reduced and ease of manufacture is improved, but the quality and consistency of single-crystalline microstructure formation deteriorates

Engineering Contradiction:
Improveease of manufactureVSAvoidmicrostructure formation quality
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

A single-crystalline substrate is provided before the additive layering process begins. This substrate serves as a predetermined nucleation site with controlled crystal orientation, enabling single-crystalline growth to initiate from a known high-quality starting point rather than forming randomly during the building process.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

Irradiation parameters (beam size, power, scan speed, exposure time) are dynamically adjusted and optimized to control the solidification process. By carefully controlling these parameters, the method achieves directional solidification and promotes epitaxial growth from the substrate, ensuring consistent single-crystalline microstructure formation throughout the work piece.

Inventive Principle:
Principle #35Parameter changes

2Device complexity

If conventional irradiation methods are used without controlled parameters, then device complexity is reduced, but the reliability of achieving single-crystalline microstructure deteriorates

Engineering Contradiction:
Improvedevice complexityVSAvoidsingle-crystalline microstructure consistency
Core Design Contradiction:
Device complexityVSReliability

Solution Approach 1:

The method implements controlled irradiation with monitored and adjusted parameters based on the crystallization behavior of the raw material powder. The system responds to the material's solidification characteristics by adapting beam parameters, ensuring that single-crystalline growth conditions are maintained throughout the building process, thereby improving reliability of microstructure formation.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

Specific irradiation parameters are optimized and controlled: beam size is adjusted to appropriate dimensions, exposure time is precisely regulated, and scan patterns are designed to promote directional solidification. These controlled parameter changes ensure reliable epitaxial growth from the substrate while avoiding unnecessary device complexity.

Inventive Principle:
Principle #35Parameter changes

3Productivity

If rapid additive layering is used to improve productivity, then production speed increases, but the quality of crystal growth and single-crystalline formation deteriorates

Engineering Contradiction:
Improveproduction speedVSAvoidcrystal growth quality
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

By pre-providing a single-crystalline substrate with controlled orientation, the method establishes a reliable nucleation foundation before additive layering begins. This allows faster building speeds because single-crystalline growth is guided from the start rather than requiring slow, controlled formation of crystal structure during the entire process.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

Irradiation parameters are optimized to enable both rapid processing and high-quality crystal growth. The beam parameters are tuned to achieve appropriate cooling rates and temperature gradients that promote directional solidification, allowing the process to maintain single-crystalline quality even at increased productivity levels.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables the reliable production of high-quality single-crystalline three-dimensional work pieces with enhanced mechanical, thermal, and chemical properties, particularly at elevated temperatures, by achieving epitaxial growth and directional solidification of dendrites along the build axis.

Implementation Method 1

The laser radiation penetrating into the powder layer causes heating and consequently melting or sintering of the raw material powder particles

Methodology Applied
Scientific EffectElectromagnetic radiation heating: Absorption (EM radiation)

Implementation Method 2

adjusting parameters such as beam size, exposure time, and crystal orientation to promote single-crystalline growth and metallurgical bonding, ensuring a consistent single-crystalline microstructure

Methodology Applied
Scientific EffectEpitaxial growth: Epitaxy

Implementation Method 3

achieving epitaxial growth and directional solidification of dendrites along the build axis

Methodology Applied
Scientific EffectDirectional solidification: Crystallisation

Data Source

PatentUS10875124B2Method, use and apparatus for producing a single-crystalline work piece
Publication Date: 2020.12.29 NIKON SLM SOLUTIONS AG
  • US10875124B2 patent drawing
  • US10875124B2 patent drawing

AI summary

A method for producing or repairing a three-dimensional work piece, the method comprising the following steps:providing at least one substrate (15);depositing a first layer of a raw material powder onto the substrate (15); andirradiating selected areas of the deposited raw material powder layer with an electromagnetic or particle radiation beam (22) in a site selective manner in accordance with an irradiation pattern which corresponds to a geometry of at least part of a layer of the three-dimensional work piece to be produced, whereinthe irradiation is controlled so as to produce a metallurgical bond between the substrate (15) and the raw material powder layer deposited thereon. Moreover, a use and apparatus are likewise disclosed.