SiOx Tridymite Carbon Coated Anode for Battery Capacity

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Solution Overview

Problem

Lithium-ion secondary batteries using silicon materials face challenges in maintaining cycle performance and battery capacity due to the expansion and contraction of silicon-based negative electrode active materials, leading to electrolyte decomposition and reduced cycle life.

Innovation Solution

A negative electrode material comprising silicon oxide (SiOx) with a tridymite structure coated with a carbon layer, where 0.5≤x≤1.6, is developed, which improves conductivity and reduces irreversible capacity through effective lithium insertion and extraction modifications.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If silicon is used as negative electrode active material to improve battery capacity, then battery capacity increases, but cycle performance deteriorates due to expansion and contraction causing particle breakage and electrolyte decomposition

Engineering Contradiction:
Improvebattery capacityVSAvoidcycle performance
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent applies nested structure by placing silicon particles inside a carbon coating layer, forming a core-shell structure where the carbon layer encapsulates the silicon active material. This nesting protects the silicon from direct contact with electrolyte while maintaining its electrochemical activity, thereby improving cycle performance without sacrificing capacity.

Inventive Principle:
Principle #7Nested doll (Nesting)

Solution Approach 2:

The patent creates a composite material system combining silicon and carbon in a specific structure. The carbon coating layer (0.5-5 μm thickness) forms a composite structure with the silicon core, providing both mechanical strength to prevent breakage and chemical stability to prevent electrolyte decomposition, while the silicon core provides high capacity.

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If silicon active material is used to increase battery capacity, then capacity improves, but electrolyte decomposition increases due to new surface creation from particle breakage

Engineering Contradiction:
Improvebattery capacityVSAvoidelectrolyte consumption
Core Design Contradiction:
Quantity of substanceVSLoss of substance

Solution Approach 1:

The patent extracts the harmful surface of silicon particles by coating them with carbon, effectively removing the direct interface between silicon and electrolyte. The carbon layer acts as a barrier that prevents electrolyte contact with the silicon surface, thereby eliminating the source of decomposition reactions while preserving the electrochemical functionality.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The carbon coating layer serves as an intermediary substance between silicon and electrolyte. It mediates the interaction by providing a stable interface that allows ionic transport while preventing direct chemical reactions between electrolyte and silicon, thus reducing electrolyte decomposition.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Reliability

If carbon coating layer is applied to silicon particles to improve cycle performance, then reliability improves, but manufacturing complexity increases

Engineering Contradiction:
Improvecycle performanceVSAvoidmanufacturing process complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent specifies precise parameter ranges for the carbon coating layer (thickness: 0.5-5 μm, carbon content: 5-50 at%) to optimize performance while managing complexity. By defining clear parameter boundaries, the invention transforms a complex manufacturing challenge into a controllable process with measurable targets.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution enhances battery performance by maintaining capacity retention and initial efficiency, preventing electrolyte decomposition, and improving the safety and electrical conductivity of the battery.

Implementation Method 1

improves conductivity of the negative electrode active material particles

Methodology Applied
Scientific EffectElectron conduction: Conduction (electrical)

Implementation Method 2

effective lithium insertion and extraction modifications

Methodology Applied
Scientific EffectLithium diffusion: Diffusion

Data Source

PatentEP3171432B1Negative electrode material for nonaqueous electrolyte secondary battery and method for producing negative electrode active material particle
Publication Date: 2020.12.16 SHIN ETSU CHEMICAL CO LTD
  • EP3171432B1 patent drawingFigure 1~2
  • EP3171432B1 patent drawingFigure 3
  • EP3171432B1 patent drawing

AI summary

The present invention is a negative electrode material for a non-aqueous electrolyte secondary battery, including negative electrode active material particles containing a silicon compound expressed by SiOx where 0.5≤x≤1.6, the silicon compound being coated with a carbon coating layer composed of a carbon component, wherein the negative electrode active material particles contain a SiO2 component having a tridymite structure and exhibit a diffraction peak around 21.825° with a half width (2θ) of 0.15° or less in X-ray diffraction. This negative electrode material for a non-aqueous electrolyte secondary battery can increase the battery capacity and improve the cycle performance and the initial charge and discharge performance.