Sliding Surface Coating With Layered Hard Carbon for Peeling Resistance

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Solution Overview

Problem

Existing sliding members, such as piston rings, face challenges in achieving both chipping resistance and wear resistance while maintaining low frictionality and peeling resistance, with existing hard carbon layer coatings falling short in providing optimal performance under high loads.

Innovation Solution

A sliding member with a coating film comprising laminated black and white hard carbon layers, where the white hard carbon layer has a higher Vickers hardness than the black hard carbon layer, and a surface layer with a lower hardness than the white hard carbon layer, optimized for friction reduction and improved adhesion, is developed. The [sp 2/(sp 2+sp 3) ratio of the layers is tailored to enhance chipping and wear resistance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If a hard carbon layer is provided to reduce friction, then low frictionality is improved, but peeling resistance deteriorates

Engineering Contradiction:
Improvelow frictionalityVSAvoidpeeling resistance
Core Design Contradiction:
Ease of operationVSStrength

Solution Approach 1:

The coating is segmented into a first hard carbon layer that provides low frictionality through its hard, lubricious surface, and a second hard carbon layer with lower hardness that provides strong adhesion and peeling resistance at the substrate interface. This segmentation resolves the contradiction between friction reduction and peeling resistance.

Inventive Principle:
Principle #1Segmentation

2Reliability

If a thick hard carbon layer is provided to improve durability, then chipping resistance and wear resistance are improved, but manufacturing complexity increases

Engineering Contradiction:
ImprovedurabilityVSAvoidcoating structure complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

Instead of forming a single thick hard carbon layer, the coating is segmented into two thinner layers with different properties. This achieves the same durability improvement while simplifying the manufacturing process, as each layer can be deposited and optimized independently with standard PVD techniques.

Inventive Principle:
Principle #1Segmentation

3Strength

If a mixed layer of hard carbon with low hardness and hard carbon with high hardness is provided to achieve both chipping resistance and wear resistance, then both properties are improved, but friction reduction and peeling resistance remain insufficient

Engineering Contradiction:
Improvechipping resistance and wear resistanceVSAvoidfriction reduction and peeling resistance
Core Design Contradiction:
StrengthVSEase of operation

Solution Approach 1:

The coating is clearly segmented into a first hard carbon layer optimized for wear resistance and a second hard carbon layer optimized for chipping resistance and adhesion. This clear segmentation, combined with specific thickness ratios and hardness differentials, ensures that friction reduction and peeling resistance requirements are met while maintaining improved chipping and wear resistance.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution provides a sliding member with enhanced chipping resistance, wear resistance, and peeling resistance, while reducing friction, particularly effective for applications under high loads, such as piston rings, by leveraging the unique properties of the laminated hard carbon layers.

Implementation Method 1

even with a physical vapor deposition (PVD) method, makes it possible to form a thick hard carbon layer having excellent durability

Methodology Applied
Scientific EffectPhysical vapor deposition: Physical Vapour Deposition

Data Source

PatentEP4316802A1Sliding member, manufacturing method thereof, and coating film
Publication Date: 2024.02.07 NIPPON PISTONRING CO LTD
  • EP4316802A1 patent drawingFigure 1~2B
  • EP4316802A1 patent drawingFigure 3A~3B
  • EP4316802A1 patent drawingFigure 4~5

AI summary

To provide a sliding member exhibiting chipping resistance and wear resistance, having excellent peeling resistance (adhesion), and realizing a reduction in friction, and a coating film. The above-described problem is solved by a sliding member (10) comprising a coating film (1) on a sliding surface (16) on a base material (11). The coating film (1) includes, when a cross section thereof is observed by a bright-field TEM image, a laminated part (1A) configured by laminating, in a thickness direction (Y), repeating units including black hard carbon layers (B), relatively shown in black, and white hard carbon layers (W), relatively shown in white, and a surface layer part (1C) composed of a white hard carbon layer provided on the laminated part (1A). A Vickers hardness of the black hard carbon layer is within a range of 700 to 1600 HV, a Vickers hardness of the white hard carbon layer is higher than a Vickers hardness of the black hard carbon layer adjacent thereto and within a range of 1200 to 2200 HV, and a Vickers hardness of the surface layer part is lower than the Vickers hardness of the white hard carbon layer and within a range of 800 to 1200 HV