Sludge Treatment with Free Ammonia for Methane Yield

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Solution Overview

Problem

Anaerobic digestion in wastewater treatment plants faces challenges in energy yield due to the elimination of primary settlers, which reduces organic carbon availability for methane production, and existing pre-treatment methods are costly and environmentally detrimental.

Innovation Solution

A method involving treating sludge with free ammonia (FA) at a pH of 8.9 or greater, with FA concentrations between 250 mg to 680 mg NH3-N/L, followed by anaerobic digestion, where part of the anaerobic digestion liquor is recirculated to maintain FA levels, reducing the need for additional chemical sources.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If the primary settler is eliminated to satisfy carbon demand for nutrient removal, then biological nutrient removal efficiency is improved, but organic carbon availability for anaerobic digestion and methane production deteriorates

Engineering Contradiction:
Improvebiological nutrient removal efficiencyVSAvoidorganic carbon availability
Core Design Contradiction:
ProductivityVSQuantity of substance

Solution Approach 1:

The invention extracts and concentrates organic carbon from the wastewater stream by eliminating the primary settler, allowing all organic carbon to proceed to the bioreactor for biomass production. The secondary sludge, which contains this concentrated organic carbon, is then subjected to pre-treatment to make it available for anaerobic digestion, effectively taking out the carbon recovery function from the traditional primary settling step.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention applies pre-treatment to secondary sludge before anaerobic digestion to break down bacterial cell walls and release intracellular organic carbon. This preliminary action transforms the poorly biodegradable secondary sludge into a form that is readily available for methane production, ensuring sufficient organic carbon supply despite the elimination of the primary settler.

Inventive Principle:
Principle #10Preliminary action

2Productivity

If pre-treatment methods are applied to secondary sludge to improve biodegradability, then methane production is enhanced, but operational costs and environmental impact increase

Engineering Contradiction:
Improvemethane productionVSAvoidoperational cost
Core Design Contradiction:
ProductivityVSEase of manufacture

Solution Approach 1:

The invention changes the chemical environment parameters by adjusting pH to alkaline conditions (pH 9-11) and controlling free ammonia concentrations (250-680 mg NH3-N/L). These parameter changes create optimal conditions for cell wall disruption and organic carbon release, enhancing subsequent methane production without requiring expensive thermal or mechanical pre-treatment methods.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses the anaerobic digestion liquor, which contains ammonia and alkalinity, as the pre-treatment agent itself. By recirculating this liquor to the pre-treatment step, the system creates a self-sustaining cycle where the digestion byproducts are reused to enhance pre-treatment, eliminating the need for external chemical additions and reducing operational costs.

Inventive Principle:
Principle #25Self-service

3Productivity

If pre-treatment is applied to secondary sludge to increase organic carbon availability, then hydrolysis rate and degradation extent improve, but chemical consumption and environmental harm worsen

Engineering Contradiction:
Improvehydrolysis rateVSAvoidenvironmental impact
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The invention converts the potentially harmful anaerobic digestion liquor, which contains ammonia and alkalinity that could cause odors or environmental issues if discharged, into a valuable pre-treatment reagent. By utilizing these components to adjust pH and free ammonia levels in the pre-treatment step, the system transforms a waste stream with potential environmental harm into a beneficial chemical agent that enhances organic carbon release.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The invention recovers valuable components (ammonia and alkalinity) from the anaerobic digestion liquor that would otherwise be discarded. By recirculating this liquor to the pre-treatment step, the system recovers these chemicals for reuse, eliminating the need for fresh chemical purchases and preventing the discharge of harmful substances, thus addressing both cost and environmental concerns.

Inventive Principle:
Principle #34Discarding and recovering

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances methane production by increasing hydrolysis rates and degradation extent, while minimizing environmental impact and operational costs by utilizing FA from anaerobic digestion liquor.

Implementation Method 1

the two basic properties that determine sludge destruction and methane production in anaerobic digestion are the hydrolysis rate and the degradation extent

Methodology Applied
Scientific EffectHydrolysis: Hydrolysis

Implementation Method 2

treating the sludge with free ammonia at a pH of 8.9 or greater, with FA concentrations between 250 mg to 680 mg NH3-N/L, followed by anaerobic digestion

Methodology Applied
Scientific EffectCell wall disruption by free ammonia:

Implementation Method 3

In the anaerobic digester, the BOD of the sludge is converted to methane

Methodology Applied
Scientific EffectAnaerobic digestion: Anaerobic Digestion

Implementation Method 4

microorganisms that catalyse these reactions grow and a substantial amount of biomass is produced

Methodology Applied
Scientific EffectBiological conversion: Fermentation

Data Source

PatentEP3580185B1Process for the treatment of sludge
Publication Date: 2024.07.24 THE UNIVERSITY OF QUEENSLAND
  • EP3580185B1 patent drawingFigure 1~2
  • EP3580185B1 patent drawingFigure 3A~3B
  • EP3580185B1 patent drawingFigure 4~5

AI summary

A method for treating a sludge derived from sewage or wastewater, the method comprising subjecting the sludge to a treatment step at a pH of 8.9 or greater and a free ammonia (FA) content of 100 mg NH3-N/L or greater. The treated sludge may be fed to a bioreactor to produce methane.