Ethylene Slurry Reactor Baffle Positioning to Prevent Pump Blockages

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Solution Overview

Problem

Continuous stirred tank reactors in ethylene slurry polymerization systems face operational interruptions due to slurry pump blockages caused by polymer lumps accumulating on reactor baffles and inner walls, leading to reduced flow and frequent cleaning needs.

Innovation Solution

The process involves maintaining the reactor liquid level above the baffle top and cooled slurry discharge point, preventing polymer deposition on baffles and mechanical supports, and using a reactor baffle system with strategically positioned baffles to minimize fouling and splashing, thereby reducing the formation of polymer lumps that could block the slurry pumps.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If cooled slurry is discharged into the vapor space above the liquid level in the reactor, then heat exchange efficiency is improved, but polymer deposition on baffles and reactor walls occurs causing pump blockages

Engineering Contradiction:
Improveheat exchange efficiencyVSAvoidslurry pump reliability
Core Design Contradiction:
TemperatureVSReliability

Solution Approach 1:

The baffle top is positioned below the liquid level before slurry discharge occurs, preventing polymer deposition on baffles and mechanical supports in advance. This preliminary positioning of the baffle eliminates the condition that leads to pump blockages while maintaining effective heat exchange through the cooled slurry discharge system

Inventive Principle:
Principle #10Preliminary action

2Temperature

If slurry is discharged above the liquid level for cooling, then cooling efficiency is improved, but polymer lumps form and block the slurry pump inlet

Engineering Contradiction:
Improvecooling efficiencyVSAvoidslurry pump flow rate
Core Design Contradiction:
TemperatureVSProductivity

Solution Approach 1:

The baffle structure is pre-positioned with its top below the liquid level to prevent polymer deposition before it occurs. This preliminary protective measure stops the formation of polymer lumps that would otherwise block the pump inlet and reduce productivity

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The baffle acts as an intermediary structure that intercepts and contains the discharged slurry within the liquid phase zone, preventing direct contact between the discharged slurry and the vapor space where polymer deposition would occur on pump inlet surfaces

Inventive Principle:
Principle #24Intermediary (Mediator)

3Reliability

If the reactor liquid level is maintained above the baffle top, then polymer deposition is prevented, but the discharge of cooled slurry may be restricted

Engineering Contradiction:
Improvepump operation reliabilityVSAvoidslurry flow rate
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The baffle is positioned at a specific location below the liquid level to create a localized zone that prevents polymer deposition on critical surfaces. This localized quality change allows the rest of the reactor to maintain normal slurry circulation and discharge flow rates

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The baffle structure is pre-positioned to prevent polymer deposition before it can occur during slurry discharge operations, ensuring reliable pump operation without restricting overall slurry flow through the reactor system

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly reduces slurry pump blockages, ensuring consistent operation by preventing polymer accumulation on reactor components and maintaining smooth slurry flow, thereby enhancing the overall performance and reliability of the ethylene slurry polymerization process.

Implementation Method 1

maintaining the reactor liquid level above the baffle top and cooled slurry discharge point

Methodology Applied
Scientific EffectLiquid level control:

Implementation Method 2

an agitator for mixing the contents of the internal reactor volume

Methodology Applied
Scientific EffectMechanical mixing: Stirring

Implementation Method 3

a reactor outlet for feeding a reactor slurry to a cooler

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Data Source

PatentEP3145632B1Process for ethylene polymerization with improved slurry pump performance
Publication Date: 2017.10.04 BASELL POLYOLEFINE GMBH
  • EP3145632B1 patent drawingFigure 1
  • EP3145632B1 patent drawingFigure 2
  • EP3145632B1 patent drawingFigure 3

AI summary

A slurry polymerization process comprising polymerizing monomers in a reactor comprising baffles, a first slurry feed line for returning cooled slurry from a cooler and optionally a second slurry feed line for transferring reactor slurry from a previous reactor of a cascade of polymerization reactors, wherein the baffle top, the first slurry feed line discharge end and the second slurry feed line end are located below the reactor liquid level.