Slurry Loop Reactor Catalyst Feed Control Around Bad Set-Point Ranges

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Solution Overview

Problem

Slurry loop reactors face reactor upsets and temperature control issues due to catalyst feed rates within the 'bad catalyst set-point range', which hinder optimal polymer production rates and quality.

Innovation Solution

A process that calculates a desired catalyst feed rate to return to optimum conditions, using a bad catalyst program to control the feed rate between established good catalyst feed rate set-points, avoiding the bad catalyst set-point range by establishing a time-weighted average feed rate.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If catalyst feed rate is increased to increase polymer production rate, then productivity is improved, but reactor upset occurs when catalyst drops enter too close together

Engineering Contradiction:
Improvepolymer production rateVSAvoidreactor stability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The control system dynamically adjusts the catalyst feed rate set-point based on real-time reactor conditions and production rate requirements. The system transitions from static set-point control to dynamic control that adapts to changing operational demands while avoiding bad catalyst set-point ranges that cause reactor upsets.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The system changes the catalyst feed rate parameter to navigate around bad set-point ranges. By adjusting the feed rate parameter dynamically and selecting alternative set-points that achieve desired production rates without entering problematic ranges, the system maintains both productivity and reactor stability.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If reactor temperature is increased to improve polymer production rate, then productivity is improved, but temperature control becomes difficult when catalyst lumps form

Engineering Contradiction:
Improvepolymer production rateVSAvoidreactor temperature control
Core Design Contradiction:
ProductivityVSTemperature

Solution Approach 1:

The control system takes preliminary action to prevent catalyst lumps from forming by avoiding bad catalyst feed rate set-points. By proactively preventing the formation of high-density catalyst pockets, the system eliminates the root cause of temperature control difficulties before they can develop.

Inventive Principle:
Principle #9Preliminary anti-action

Solution Approach 2:

The system uses feedback from production rate measurements and reactor monitoring to continuously adjust catalyst feed rate decisions. This closed-loop control enables the system to respond to changing conditions and maintain stable temperature control while optimizing production rate.

Inventive Principle:
Principle #23Feedback

3Productivity

If catalyst feed rate is adjusted to optimize production rate, then productivity is improved, but manufacturing precision deteriorates when entering bad catalyst set-point range

Engineering Contradiction:
Improvepolymer production rateVSAvoidcatalyst feed rate control precision
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The control system segments the catalyst feed rate range into good and bad set-point zones. By identifying and avoiding bad catalyst set-point ranges while utilizing good ranges, the system maintains precise control over catalyst feed rate while optimizing production rate.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The system dynamically selects catalyst feed rate set-points from available good ranges based on current production requirements. This dynamic selection process maintains manufacturing precision by continuously choosing optimal set-points that avoid bad ranges while achieving desired production rates.

Inventive Principle:
Principle #15Dynamics

Data Source

PatentUS11813583B2Slurry loop reactor bad catalyst range control
Publication Date: 2023.11.14 EXXONMOBIL CHEMICAL PATENTS INC
  • US11813583B2 patent drawing
  • US11813583B2 patent drawing

AI summary

A process for maintaining an optimum polymerization process in a continuous loop polymerization reactor by driving a catalyst feed range set-point around a bad catalyst set-point range using a bad catalyst feed rate program to vary the catalyst feed rate for differing periods of time between previously determined good catalyst feed rates.