Alkaline-Earth Halide Scintillator Sm2+ Co-Doping

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Solution Overview

Problem

Existing scintillators face challenges in achieving large volume with minimal self-absorption, which affects energy resolution, and often contain radioactive isotopes that interfere with precise radiation measurements.

Innovation Solution

A crystalline alkaline earth halide scintillator doped with Samarium (Sm2+) is co-doped to shift the scintillation emission wavelength beyond 670 nm, reducing self-absorption and eliminating intrinsic radioactivity, allowing for high light intensity and transparency to its own emitted light.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Illumination intensity

If rare earth halides such as LaBr3:Ce or LaCl3:Ce are used as scintillators, then high light intensity is achieved, but radioactive isotopes interfere with precise radiation measurements

Engineering Contradiction:
Improvelight intensityVSAvoidradioactive interference
Core Design Contradiction:
Illumination intensityVSObject-affected harmful factors

Solution Approach 1:

The invention changes the chemical composition parameters by using alkaline earth halides (SrI2, BaI2, CaI2) instead of rare earth halides, and by co-doping with specific concentrations of Sm2+ (0.1-5 mol%) and Eu2+ (0.1-5 mol%). This parameter change eliminates intrinsic radioactivity while maintaining high light intensity through the activator-doped crystal structure.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a composite scintillator material by combining alkaline earth halide matrix with multiple dopants (Sm2+ and Eu2+). This composite approach allows the material to achieve both low radioactivity (from the alkaline earth base) and high light intensity (from the activator dopants), resolving the contradiction between these two properties.

Inventive Principle:
Principle #40Composite materials

2Volume of moving object

If scintillator volume is increased to greater than 1 cm3 for effective radiation detection, then detection capability is improved, but self-absorption of emitted light increases

Engineering Contradiction:
Improvescintillator volumeVSAvoidself-absorption
Core Design Contradiction:
Volume of moving objectVSLoss of energy

Solution Approach 1:

The invention changes the optical parameter by shifting the emission wavelength to beyond 670 nm through Sm2+ co-doping. This wavelength shift reduces the overlap between emission spectrum and absorption spectrum, thereby reducing self-absorption losses and enabling large volume scintillators to maintain high light transmission efficiency.

Inventive Principle:
Principle #35Parameter changes

3Loss of energy

If emission wavelength is shifted beyond 670 nm through Sm2+ co-doping, then self-absorption is reduced, but photodetector sensitivity requirements increase

Engineering Contradiction:
Improveself-absorption lossVSAvoidphotodetector sensitivity requirement
Core Design Contradiction:
Loss of energyVSDevice complexity

Solution Approach 1:

The invention optimizes the emission wavelength parameter to the range beyond 670 nm (specifically 750-850 nm for Sm2+). While this requires photodetectors sensitive to these wavelengths (such as red-extended PMTs or SiPMs), the significant reduction in self-absorption losses more than compensates for the photodetector requirement, resulting in net improved detection efficiency.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution results in a scintillator with improved energy resolution and reduced self-absorption, enabling precise ionizing radiation detection without interference from intrinsic radioactivity, using a photodetector sensitive to the shifted emission wavelength.

Implementation Method 1

The scintillator material receives ionizing radiation, which causes it to emit scintillation light

Methodology Applied
Scientific EffectScintillation: Scintillation

Implementation Method 2

Rare earth halides such as LaBr3:Ce or LaCl3:Ce... are scintillators with high light intensity

Methodology Applied
Scientific EffectPhotoluminescence: Photoluminescence

Implementation Method 3

The scintillators used may in particular be made of a single crystal of sodium iodide doped with thallium... cesium iodide doped with thallium or sodium... which is then transformed into an electrical signal using a photodetector such as a photomultiplier

Methodology Applied
Scientific EffectPhotoelectric Effect: Photoelectric Effect

Data Source

PatentEP3737732B1Scintillator material comprising a crystalline alkaline-earth halide doped with an activator and co-doped with sm2+
Publication Date: 2022.06.01 STICHTING VOOR DE TECH WETENSCHAPPEN
  • EP3737732B1 patent drawingFigure 1~2
  • EP3737732B1 patent drawingFigure 3~4
  • EP3737732B1 patent drawingFigure 5

AI summary

The invention relates to a scintillator material for an ionising radiation detector, comprising a crystalline alkaline-earth halide including at least one alkaline earth selected from among Mg, Ca, Sr, Ba, said alkaline-earth halide being doped with at least one scintillation activator dopant different from Sm2+, and co-doped with Sm2+, said alkaline-earth halide comprising at least one halide selected from among Br, Cl, I.