Sodium Bicarbonate Production via On-Site CO2 Capture

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Solution Overview

Problem

Current industrial processes for producing sodium bicarbonate are inefficient, introduce impurities, and rely on external carbon dioxide sources, leading to quality control issues and environmental concerns, particularly in food and medical applications.

Innovation Solution

A method that utilizes low-carbon dioxide product streams from carbonaceous feedstock treatment, capturing and reacting the CO2 with sodium carbonate to produce high-purity sodium bicarbonate, while also utilizing heat for energy efficiency and reducing waste, integrating carbon capture and bicarbonate synthesis in a single process.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If commercial sources of carbon dioxide are used, then high purity sodium bicarbonate can be produced, but logistical challenges and high costs arise for transport and storage

Engineering Contradiction:
Improvepurity of sodium bicarbonateVSAvoidlogistical complexity for CO2 transport and storage
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent uses an ammonia-soda process plant as an intermediary system to generate carbon dioxide on-site from calcium carbonate decomposition, eliminating the need for external CO2 transport and storage infrastructure while maintaining product purity through controlled reaction conditions

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The system generates its own carbon dioxide feedstock by decomposing calcium carbonate in kilns, making the process self-sufficient regarding CO2 supply and eliminating dependence on external commercial sources or complex logistics chains

Inventive Principle:
Principle #25Self-service

2Productivity

If kiln gas from ammonia-soda process is used, then sodium bicarbonate can be produced, but impurities are introduced affecting quality control

Engineering Contradiction:
Improveproduction of sodium bicarbonateVSAvoidquality control and purity of sodium bicarbonate
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent extracts only the carbon dioxide component from the kiln gas stream by capturing it from the flue gas, separating it from other impurities such as nitrogen and sulfur compounds, thereby achieving high purity sodium bicarbonate production while maintaining efficient carbon utilization

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The system controls the composition and purity of carbon dioxide by adjusting combustion parameters in the kilns and using solvent capture processes to selectively remove CO2 from the flue gas, ensuring consistent product quality despite variations in feedstock

Inventive Principle:
Principle #35Parameter changes

3Quantity of substance

If low CO2 content product streams are used, then previously unused CO2 sources can be utilized, but the efficiency of sodium bicarbonate production is reduced

Engineering Contradiction:
Improveutilization of CO2 from previously unused sourcesVSAvoidefficiency of sodium bicarbonate production
Core Design Contradiction:
Quantity of substanceVSProductivity

Solution Approach 1:

The patent implements continuous carbon dioxide capture from low-concentration flue gas streams using solvent absorption towers operating in continuous mode, maintaining steady production rates despite the low CO2 concentration in the feed gas by processing large volumes continuously

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The system serves multiple functions simultaneously: generating heat for process requirements, producing carbon dioxide for sodium bicarbonate synthesis, and capturing CO2 from low-concentration streams that would otherwise be vented, thereby efficiently utilizing previously wasted resources

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables the production of high-purity sodium bicarbonate from previously unused CO2 sources, reduces energy demand, and minimizes environmental impact by recycling heat and water, thus improving the overall efficiency and sustainability of the process.

Implementation Method 1

treating a carbonaceous feedstock to form a product stream comprising up to 10 v/v% carbon dioxide

Methodology Applied
Scientific EffectCombustion: Combustion

Implementation Method 2

capturing at least a portion of the carbon dioxide from the product stream to form a carbon dioxide stream

Methodology Applied
Scientific EffectAbsorption: Absorption (physical)

Implementation Method 3

contacting at least a portion of the carbon dioxide stream with at least a portion of the aqueous sodium carbonate solution to form a slurry comprising solid sodium bicarbonate

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 4

separating the solid component of the slurry from the liquid component of the slurry to provide solid sodium bicarbonate and an aqueous liquor

Methodology Applied
Scientific EffectSedimentation: Sedimentation

Data Source

PatentEP3844107B1Sodium bicarbonate production
Publication Date: 2024.04.10 TATA CHEM EURO LTD
  • EP3844107B1 patent drawingFigure 1
  • EP3844107B1 patent drawingFigure 2
  • EP3844107B1 patent drawingFigure 3

AI summary

The present invention relates to a method for the production of sodium bicarbonate, particularly for producing sodium bicarbonate on an industrial scale, the method comprising the steps of: a. treating a carbonaceous feedstock to form a product stream comprising up to 10 v/v% carbon dioxide; b. capturing at least a portion of the carbon dioxide from the product stream to form a carbon dioxide stream; c. feeding the carbon dioxide stream to a reaction vessel; d. feeding an aqueous sodium carbonate solution to the reaction vessel; e. contacting at least a portion of the carbon dioxide stream with at least a portion of the aqueous sodium carbonate solution to form a slurry comprising solid sodium bicarbonate; and f. separating the solid component of the slurry from the liquid component of the slurry to provide solid sodium bicarbonate and an aqueous liquor.