Sodium Bicarbonate Fluid Bed Cooling for Flowability

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Solution Overview

Problem

Sodium bicarbonate powders tend to cake and have poor flow characteristics, especially under ambient storage conditions of temperature and relative humidity, leading to stability issues and agglomeration, which affects their usability in applications such as animal feed and flue gas treatment.

Innovation Solution

A process involving a fluid bed cooling unit where dried sodium bicarbonate solids are cooled to an outlet temperature of 95° F. or less, using a fluidization gas stream that may include CO2, and classifying the product to generate different particle sizes, enhancing its flowability and stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If sodium bicarbonate is produced by conventional drying and storage methods, then production cost is reduced, but the product tends to cake and has poor flow characteristics under ambient storage conditions

Engineering Contradiction:
Improveproduction costVSAvoidflowability
Core Design Contradiction:
Ease of manufactureVSEase of operation

Solution Approach 1:

The patent applies parameter changes by controlling the outlet temperature of the drying apparatus to be 95°F or less, and by introducing a fluidization gas stream at a controlled temperature and flow rate. These parameter changes prevent thermal degradation and maintain particle flowability while avoiding the need for expensive additives or complex processing steps

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses a fluidization gas stream (pneumatic method) to fluidize the dried sodium bicarbonate solids in a fluid bed cooling unit. This pneumatic approach enhances heat transfer, prevents caking, and maintains excellent flowability by keeping particles suspended and preventing compaction, without requiring additional flow aids

Inventive Principle:
Principle #29Pneumatics and hydraulics

2Ease of operation

If sodium bicarbonate is stored under ambient conditions, then storage simplicity is improved, but the product decomposes and cakes due to high humidity and temperature

Engineering Contradiction:
Improvestorage simplicityVSAvoidstability
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The patent applies preliminary action by drying the sodium bicarbonate to a controlled outlet temperature of 95°F or less before storage. This preliminary cooling and drying step prevents subsequent thermal degradation and caking during ambient storage, ensuring long-term stability without requiring controlled storage conditions or additives

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent introduces a fluidization gas stream that creates a controlled atmospheric environment during drying and cooling. This gas atmosphere prevents moisture absorption and thermal degradation, effectively creating an inert-like protective environment that maintains product stability during ambient storage

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

3Ease of operation

If sodium bicarbonate particles are cooled to lower temperatures, then flowability is improved, but energy consumption increases

Engineering Contradiction:
ImproveflowabilityVSAvoidenergy consumption
Core Design Contradiction:
Ease of operationVSUse of energy by moving object

Solution Approach 1:

The patent optimizes the cooling parameter by setting the outlet temperature to 95°F or less, which is sufficient to prevent caking and maintain flowability without excessive energy consumption. This parameter optimization balances flowability improvement with energy efficiency

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses the fluidization gas stream to provide both cooling and fluidization functions simultaneously. The pneumatic fluidization enhances heat transfer efficiency, allowing effective cooling at lower energy consumption by maximizing the heat transfer coefficient through particle suspension and increased surface area exposure

Inventive Principle:
Principle #29Pneumatics and hydraulics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process results in a particulate sodium bicarbonate product with improved flowability and stability, maintaining free-flowing properties even under ambient storage conditions, reducing the likelihood of caking and agglomeration, and enhancing its suitability for various applications.

Implementation Method 1

flowing a fluidization gas stream in the fluid bed cooling unit to fluidize the dried sodium bicarbonate solids

Methodology Applied
Scientific EffectFluidization: Fluidisation

Implementation Method 2

adjusting the temperature of the cooling fluid flowing through the at least one cooling element in order for the sodium bicarbonate product to have an outlet temperature of 95° F. or less

Methodology Applied
Scientific EffectHeat transfer: Conduction (thermal)

Data Source

PatentUS10392257B2Method for enhancing sodium bicarbonate flowability
Publication Date: 2019.08.27 SOLVAY SA
  • US10392257B2 patent drawing
  • US10392257B2 patent drawing

AI summary

A process for producing crystalline sodium bicarbonate, comprising: feeding dried sodium bicarbonate solids with a mass flow rate to a fluid bed cooling unit, wherein said cooling unit comprises at least one cooling element through which flows a cooling fluid; flowing a fluidization gas stream in the fluid bed cooling unit to fluidize the dried sodium bicarbonate solids, in order for the dried sodium bicarbonate solids to be in thermal contact with the at least one cooling element; withdrawing a sodium bicarbonate product from the fluid bed cooling unit; and adjusting the temperature of the cooling fluid flowing through the at least one cooling element in order for the sodium bicarbonate product to have an outlet temperature of 95° F. or less, preferably less than 90° F., when being withdrawn from the fluid bed cooling unit.