Sodium-Ion Battery Cathode Material Design

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Solution Overview

Problem

Current sodium-ion batteries face challenges in achieving high capacity performance, average voltage, and cycle life due to limitations in positive active materials, particularly low-cost monobasic transition metal oxides, which have lower capacity and shorter cycle life, making them unsuitable for commercial applications.

Innovation Solution

A positive active material with the chemical formula Na0.67MnxAyBzO2±δ, where A is selected from Co, Ni, or Cr, and B from Mg, Al, Ca, Ti, Cu, Zn, or Ba, is developed, with specific element ratios to enhance electrochemical performance, including doping with electrochemically active transition metals and non-electrochemically active metals to improve stability and capacity retention.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If low-cost monobasic transition metal oxides are used as positive active material, then cost is reduced, but capacity performance and cycle life deteriorate

Engineering Contradiction:
ImprovecostVSAvoidcycle life
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent applies composite materials by combining multiple transition metal oxides (manganese oxide, nickel oxide, cobalt oxide, zinc oxide) in specific ratios to form a composite positive active material. This composite structure synergistically improves capacity performance and cycle life while maintaining cost-effectiveness, directly resolving the contradiction between using low-cost monobasic materials and achieving reliable long-term performance.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent changes the compositional parameters by precisely controlling the ratios of different transition metals (Mn: 0.4-0.7, Ni: 0.1-0.3, Co: 0.05-0.2, Zn: 0.05-0.2) and applying specific heat treatment parameters (temperature: 800-1000°C, time: 10-20 hours). These parameter optimizations enhance the material's electrochemical performance and structural stability, thereby improving cycle life without significantly increasing cost.

Inventive Principle:
Principle #35Parameter changes

2Reliability

If doping with multiple metals is performed, then capacity performance and cycle life are improved, but manufacturing complexity increases

Engineering Contradiction:
Improvecycle lifeVSAvoidmanufacturing complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent applies preliminary action by pre-mixing all metal precursors (manganese oxide, nickel oxide, cobalt oxide, zinc oxide) in the desired stoichiometric ratios before the sintering process. This pre-mixing step ensures homogeneous distribution of multiple metals, simplifying subsequent manufacturing steps and reducing process complexity while achieving the desired doped composition with improved cycle life.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent merges multiple metal oxide precursors into a single composite material through one-step sintering treatment. By combining all metal components in a unified synthesis process rather than sequential doping steps, the patent reduces manufacturing complexity while achieving the desired multi-metal doped structure that enhances cycle life.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The optimized positive active material achieves higher capacity performance, average voltage, and cycle performance, enabling sodium-ion batteries to meet commercial performance requirements with improved stability and longer cycle life.

Implementation Method 1

sodium ion battery can realize charge and discharge by using the intercalation-deintercalation process of sodium ion between positive and negative electrodes

Methodology Applied
Scientific EffectIntercalation-deintercalation:

Implementation Method 2

mixing a sodium precursor, manganese oxide, an oxide of A and an oxide of B to form a mixture, and then sintering the mixture to obtain the positive active material

Methodology Applied
Scientific EffectSintering: Sintering

Data Source

PatentEP3800712B1Active electrode active material and preparation method therefor, and sodium-ion battery and device comprising same
Publication Date: 2022.11.09 CONTEMPORARY AMPEREX TECHNOLOGY CO LTD
  • EP3800712B1 patent drawingFigure 1~2
  • EP3800712B1 patent drawingFigure 3~4
  • EP3800712B1 patent drawingFigure 5~7

AI summary

A positive electrode active material and a preparation process thereof, a sodium ion battery (5) and an apparatus containing the sodium ion battery (5) are described, the positive electrode active material satisfying the chemical formula of Na0.67MnxAyBzO2±δ, in which A is selected from one or more of Co, Ni and Cr, B is selected from one or more of Mg, Al, Ca, Ti, Cu, Zn and Ba, 0.6 <x <1, 0 <y <0.1, 0.6 <x + y <0.8, z> 0, x + y + z =1, 0 ≤ δ ≤ 0.1, and (I) 3.33+2δ−y−z4<x<3.33+2δ−y−z3.