Solid Oxide Fuel Cell Gel Cast Process Warping Reduction

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Solution Overview

Problem

The existing manufacturing method for solid oxide fuel cells (SOFCs) results in increased electric resistance and limited design freedom for fuel channels due to large particle sizes and susceptibility to warping, leading to reduced output density and potential damage during the sintering process.

Innovation Solution

The method involves using a gel cast process with ceramic slurry containing ceramic powder, dispersion media, and a gelling agent to form compacts with smaller primary particles, allowing for increased contact area and reduced warping by accommodating the support-member divided-member in a different molding die for forming the solid electrolyte and fuel-side electrode, thereby enhancing electrical connection and design flexibility.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If press molding with secondary particles is used to form the support member, then the degree of freedom in fuel channel shape is increased, but the particle size becomes large (about 80 μm) resulting in reduced contact area and increased electric resistance

Engineering Contradiction:
Improvedegree of freedom in fuel channel shapeVSAvoidelectrical connection quality
Core Design Contradiction:
Adaptability or versatilityVSReliability

Solution Approach 1:

The invention changes the particle size parameter from large secondary particles (about 80 μm) to fine primary particles (about 1-10 μm) by using spray-dried powder instead of granular secondary particles in the press molding process. This parameter change increases the contact area between the support member and fuel-side electrode, thereby reducing electric resistance and improving electrical connection quality while maintaining the ability to form complex fuel channel shapes.

Inventive Principle:
Principle #35Parameter changes

2Adaptability or versatility

If two compacts of support-member divided-member are bonded before sintering, then complicated fuel channel shapes can be formed, but the unbonded compact is susceptible to warping and cracking during subsequent processing

Engineering Contradiction:
Improvefuel channel shape complexityVSAvoidstructural integrity during processing
Core Design Contradiction:
Adaptability or versatilityVSStrength

Solution Approach 1:

The invention applies preliminary sintering to the bonded compact of support-member divided-members before forming the fuel-side electrode and solid electrolyte compacts. This preliminary sintering action strengthens the bonded compact, preventing warping and cracking during subsequent handling and processing steps, while still allowing the formation of complicated fuel channel shapes through the bonded divided-members.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach reduces the electric resistance of the SOFCs, increases output density, and prevents warping of the support member, resulting in a more efficient and robust fuel cell with improved electrical performance and design flexibility.

Implementation Method 1

a gel cast process with ceramic slurry containing ceramic powder, dispersion media, and a gelling agent to form compacts with smaller primary particles

Methodology Applied
Scientific EffectGelation: Gel

Data Source

PatentEP2518808B1Method for producing solid oxide fuel cell and method for producing divided solid oxide fuel cell molded product
Publication Date: 2017.03.22 NGK INSULATORS LTD
  • EP2518808B1 patent drawingFigure 1~2
  • EP2518808B1 patent drawingFigure 3
  • EP2518808B1 patent drawingFigure 4

AI summary

A compact of a support-member divided-member, which has a shape formed by dividing a support member into two in the thickness direction so as to divide the fuel channel into two in the thickness direction, is manufactured by a gel cast method in which slurry is filled in a molding die. A compact of a fuel-side electrode and a compact of an electrolyte are successively stacked on the upper surface of the compact of the support-member divided-member, whereby a compact of a cell divided member is obtained. The two compacts of the cell divided member are bonded and sintered, whereby an SOFC cell (sintered body) in which an oxygen-side electrode is not formed is formed. A compact of the oxygen-side electrode is formed respectively on the upper and lower surfaces of the sintered body, and then, the compact of the oxygen-side electrode is sintered, whereby the SOFC cell is completed.