Sol-Gel Cookware Coating for Heat-Stable Easy Cleaning

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Solution Overview

Problem

Existing cookware coatings, such as PTFE and ceramic coatings, fail to provide effective stain, abrasion, and thermal resistance, are difficult to clean, and may release harmful substances when exposed to high temperatures, while multi-layer coatings increase production costs and health risks.

Innovation Solution

A sol-gel coated metalware with a monolayer composition of dimethyl siloxane, tetraethoxysilane, amorphous silicon dioxide, and inorganic pigments, catalyzed by 1-ethyl-3-methylimidazolium methyl sulfate, applied directly to the metallic surface without additional interlayers, offering a cost-effective and health-safe solution for elevated temperature applications.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If PTFE coating is applied to provide non-sticking properties, then ease of cleaning is improved, but abrasion resistance deteriorates and the coating loses form and position when rubbed with sharp metal objects

Engineering Contradiction:
Improveease of cleaningVSAvoidabrasion resistance
Core Design Contradiction:
Ease of operationVSStrength

Solution Approach 1:

The patent changes the material parameters by using a cross-linked polymer matrix with specific glass transition temperature (Tg) and melting temperature (Tm) ranges, along with controlled particle size distribution (5-50 micrometers) of inorganic fillers, to achieve both non-stick and abrasion-resistant properties simultaneously

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The coating is formulated as a composite material combining organic polymer components (resin, cross-linking agents) with inorganic fillers (metal oxides, ceramic particles), creating a synergistic effect where the organic matrix provides non-stick properties and the inorganic phase provides abrasion resistance

Inventive Principle:
Principle #40Composite materials

2Ease of operation

If PTFE coating is used to provide non-sticking properties, then ease of cleaning is improved, but thermal stability deteriorates as PTFE undergoes pyrolysis at 200°C and decomposes at 350°C releasing harmful gases

Engineering Contradiction:
Improveease of cleaningVSAvoidthermal stability
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The patent raises the thermal stability parameters by selecting polymer matrices with Tg > 80°C and Tm > 150°C, and inorganic fillers with high melting points, enabling the coating to withstand temperatures up to 400°C without decomposition or harmful gas release

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces the thermally unstable PTFE material with thermally stable alternative materials that maintain their structural integrity and non-stick properties at high cooking temperatures, eliminating the need to discard the coating after thermal degradation

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Strength

If anodification step is added to establish aluminum oxide layer for ceramic coating, then adhesion is improved, but production costs increase

Engineering Contradiction:
ImproveadhesionVSAvoidproduction cost
Core Design Contradiction:
StrengthVSEase of manufacture

Solution Approach 1:

The patent incorporates adhesion promoters and surface preparation agents directly into the coating formulation, allowing the coating to self-adhere to aluminum surfaces without requiring preliminary anodification treatment, thus eliminating the additional production step

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent extracts and eliminates the anodification step from the manufacturing process by using alternative adhesion mechanisms through chemical modifiers and coupling agents in the coating composition that provide sufficient bonding without the complex multi-step anodization process

Inventive Principle:
Principle #2Taking out (Extraction)

4Reliability

If multiple coating layers are applied to achieve desired properties, then performance is improved, but device complexity and production costs increase

Engineering Contradiction:
Improvecoating performanceVSAvoidnumber of process steps
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent merges multiple functional components (adhesion promoters, non-stick agents, abrasion-resistant fillers, thermal stabilizers, coloring pigments) into a single integrated coating composition that provides all desired properties in one application step, eliminating the need for multiple sequential coating layers

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The coating formulation is designed as a universal multi-functional composition where a single coating layer simultaneously provides adhesion, non-stick properties, abrasion resistance, thermal stability, and aesthetic appearance, replacing the need for specialized separate layers for each function

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The sol-gel coated metalware achieves excellent stain, abrasion, and thermal resistance, ease of cleaning, and maintains performance at high temperatures without the need for additional oxide layers or multiple process steps, ensuring safety and cost-effectiveness.

Implementation Method 1

a coating which is a hydrolysis and polycondensation product of a composition

Methodology Applied
Scientific EffectHydrolysis: Hydrolysis

Implementation Method 2

a coating which is a hydrolysis and polycondensation product of a composition

Methodology Applied
Scientific EffectPolycondensation:

Implementation Method 3

catalyzed by 1-ethyl-3-methylimidazolium methyl sulfate

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 4

thermally-stable... maintains performance at high temperatures... resistant, easy-to-clean layer formation for coating of metalware surfaces for use in elevated temperatures

Methodology Applied
Scientific EffectThermal stability:

Data Source

PatentEP2803302B1Chemically stable, stain-, abrasion- and temperature-resistant, easy-to-clean sol-gel coated metalware for use in elevated temperatures
Publication Date: 2015.12.30 EKSEN MAKINE SANAYI & TICARET
  • EP2803302B1 patent drawingFigure 1

AI summary

A metalware for use in elevated temperatures, where the surface of the said ware is coated with a layer which is a hydrolysis and polycondensation product of a composition comprising tetraethoxy silane (TEOS), methyl trimethoxy silane (MTMS), dimethyl siloxane (DMS), inorganic filler and polar solvent where the said composition comprises 1,3-dialkyl imidazolium alkyl sulfate.