Solid Oxide Cell Barrier Layer Against La2Zr2O7 Resistance

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Solution Overview

Problem

The formation of high resistance phases such as La2Zr2O7 during the manufacture of solid oxide electrochemical cells can lead to deteriorated cell performance, especially when using lanthania-cobalt based oxides for oxygen electrodes and zirconia-based electrolytes.

Innovation Solution

A porous barrier-layer made of doped ceria with a thickness of 100µm or greater and 500µm or less and a porosity of greater than 10% is introduced between the electrolyte and the oxygen electrode to prevent the formation of high resistance phases.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If LaCoO3-based oxide is used for the oxygen electrode to achieve higher electric conductivity and catalytic activity, then the electrode performance is improved, but the reactivity with ZrO2-based electrolyte increases leading to high resistance phase formation

Engineering Contradiction:
Improveelectrode performanceVSAvoidhigh resistance phase formation
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent introduces a porous barrier-layer made of doped ceria as an intermediary layer between the LaCoO3-based oxygen electrode and the ZrO2-based electrolyte. This intermediary layer physically separates the two reactive materials, preventing direct contact and the formation of high resistance phases (such as La2Zr2O7) while still allowing ionic transport necessary for cell operation.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The implementation of the porous barrier-layer effectively suppresses the diffusion of components between the electrolyte and the oxygen electrode, thereby improving the cell performance by maintaining high current density and reducing pressure loss.

Implementation Method 1

suppresses the diffusion of components between the electrolyte and the oxygen electrode

Methodology Applied
Scientific EffectDiffusion: Diffusion

Data Source

PatentEP3933986B1Electrochemical cell and electrochemical cell stack
Publication Date: 2025.05.21 TOSHIBA ENERGY SYST & SOLUTIONS CORP
  • EP3933986B1 patent drawingFigure 1
  • EP3933986B1 patent drawingFigure 2A~2D
  • EP3933986B1 patent drawingFigure 3

AI summary

An electrochemical cell according to an embodiment includes a hydrogen electrode, an electrolyte laminated on the hydrogen electrode, a barrier-layer laminated on the electrolyte, and an oxygen electrode laminated on the barrier-layer. The barrier-layer has a porous structure having a thickness of greater than 20 µm and a porosity of greater than 10%.